Photomoisture curable resin composition, adhesive for electronic parts, and adhesive for display elements
A resin composition, moisture curing technology, applied in the direction of adhesives, polyurea/polyurethane adhesives, adhesive types, etc., can solve the problems of insufficient adhesive reliability, creep resistance, etc.
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Synthetic example 1
[0140] (Synthesis example 1 (production of urethane prepolymer A))
[0141] 100 parts by weight of polytetramethylene ether glycol (manufactured by Mitsubishi Chemical Corporation, "PTMG-2000") and 0.01 part by weight of dibutyltin dilaurate as a polyol compound were put into a separable flask with a volume of 500 mL. , under vacuum (20mmHg or less), stirred at 100° C. for 30 minutes, and mixed. Thereafter, under normal pressure, 26.5 parts by weight of diphenylmethane diisocyanate (manufactured by Nisso Shoji Co., Ltd. "PureMDI") was added as a polyisocyanate compound, stirred at 80° C. for 3 hours, and reacted to obtain a urethane prepolymer. Material A (weight average molecular weight 2700).
Synthetic example 2
[0142] (Synthesis example 2 (production of urethane prepolymer B))
[0143] 100 parts by weight of polypropylene glycol (manufactured by Asahi Glass Co., Ltd. "EXCENOL 2020") and 0.01 part by weight of dibutyltin dilaurate as a polyol compound were put into a separable flask with a capacity of 500 mL. °C for 30 minutes for mixing. Thereafter, under normal pressure, 26.5 parts by weight of diphenylmethane diisocyanate (manufactured by Nisso Shoji Co., Ltd. "Pure MDI") was added as a polyisocyanate compound, stirred at 80° C. for 3 hours, and reacted to obtain a urethane precursor. Polymer B (weight average molecular weight 2900).
Synthetic example 3
[0144] (Synthesis example 3 (production of urethane prepolymer C))
[0145] In a reaction vessel containing the urethane prepolymer A obtained in the same manner as in Synthesis Example 1, 1.3 parts by weight of hydroxyethyl methacrylate and N-nitrosophenylhydroxylamine as a polymerization inhibitor were added. 0.14 parts by weight of aluminum salt (manufactured by Wako Pure Chemical Industries, Ltd., "Q-1301") was stirred and mixed for 1 hour at 80°C under a nitrogen stream to obtain a urethane prepolymer having isocyanate groups and methacryloyl groups at molecular terminals. C (weight average molecular weight 2900).
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