A reactive hot melt adhesive composition and its preparation method and application
A technology of hot-melt adhesives and compositions, applied in the direction of adhesive types, polyurea/polyurethane adhesives, polymer adhesive additives, etc., to achieve the effect of increasing the reaction speed and the depth of colloid curing
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Embodiment 1
[0042] Take 80g of isocyanate prepolymer A, 10g of tackifying resin, 1g of fumed silica (R972), 9g of silane-modified silicone resin D, and 0.02g of toluenesulfonyl isocyanate into the reaction kettle. At 80°C, vacuumize and mix for 60min. Add 0.10g of γ-aminopropyltrimethoxysilane (KH-540), a mixture of stannous octoate and 2'2-dimorpholinodiethyl ether (1:1) 0.1g. After vacuum mixing for 15 minutes. Vacuum defoaming for 30min. Glue out. Pour into the mold to measure the curing depth and shear strength test.
Embodiment 2
[0044] Take 70g of isocyanate prepolymer A, 10g of tackifying resin, 1g of fumed silica (R972), 19g of silane-modified silicone resin D, and 0.02g of toluenesulfonyl isocyanate into the reaction kettle. At 80°C, vacuumize and mix for 60min. Add 0.20g of γ-aminopropyltrimethoxysilane (KH-540), a mixture of stannous octoate and 2'2-dimorpholinodiethyl ether (1:1) 0.1g. After vacuum mixing for 15 minutes. Vacuum defoaming for 30min. Glue out. Pour into the mold to measure the curing depth and shear strength test.
Embodiment 3
[0046] Take 60g of isocyanate prepolymer A, 10g of tackifying resin, 1g of fumed silica (R972), 29g of silane-modified silicone resin D, and 0.02g of toluenesulfonyl isocyanate into the reaction kettle. At 80°C, vacuumize and mix for 60min. Add 0.30g of γ-aminopropyltrimethoxysilane (KH-540), a mixture of stannous octoate and 2'2-dimorpholinodiethyl ether (1:1) 0.1g. After vacuum mixing for 15 minutes. Vacuum defoaming for 30min. Glue out. Pour into the mold to measure the curing depth and shear strength test.
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