Method for extracting and purifying humus in soil, peat and lignite
A purification method and technology for humic substances, which are applied in the field of humic acid extraction technology, can solve the problems of increasing the difficulty and cost of extraction, unable to meet the production needs of industrialization, and unfavorable for the industrialization of various components of humic substances.
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[0082] Such as figure 2 Shown, a kind of extraction and purification method applicable to humus in soil, peat and lignite, comprises the following steps:
[0083] (Ⅰ) Alkaline extraction of DOM
[0084] (ⅰ) DOM extraction
[0085] (A) Dosing
[0086] (1) Alkaline extract (0.1mol / L): Na 4 P 2 o 7 +NaOH (molar ratio 1:1) solution
[0087] Weigh 265.90g anhydrous Na 4 P 2 o 7 Dissolve with 40.00g NaOH and make to 20L solution;
[0088] Configure Na every time 4 P 2 o 7 +NaOH (molar ratio 1:1) needs to measure the pH value, measure the pH after cooling the extract solution to room temperature each time, and compare the change of pH value before and after adding the extract solution.
[0089] (2) 1:1 hydrochloric acid
[0090] Measure 12L of concentrated hydrochloric acid (4 bottles x 3L / bottle) and set the volume to 24L;
[0091] (B) extract
[0092] (1) Weigh 400g of black soil that has been air-dried and passed through a 100-mesh sieve into a 2L polytetrafluoro ...
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