Electrochemical sensing electrode based on flower-like zinc oxide@ferrocene functionalized three-dimensional graphene
A flower-shaped zinc oxide and sensing electrode technology, which is applied in the field of electrochemical sensing electrodes, can solve the problems of poor sensitivity and slow detection speed, and achieve the effect of improving electrocatalytic performance
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specific Embodiment approach 1
[0023] Specific embodiment one: A kind of electrochemical sensing electrode based on flower-shaped zinc oxide@ferrocene functionalized three-dimensional graphene in this embodiment is characterized in that it is based on a flower-shaped zinc oxide@ferrocene functionalized three-dimensional graphite The electrochemical sensing electrode of ene is composed of a GCE electrode and a three-dimensional graphene composite based on flower-like ZnO@ferrocene functionalization wrapped around the GCE electrode.
specific Embodiment approach 2
[0024] Specific embodiment 2: The difference between this embodiment and specific embodiment 1 is that the electrochemical sensing electrode based on flower-like zinc oxide@ferrocene functionalized three-dimensional graphene is characterized in that the flower The zinc oxide nanosheets are intercalated by zinc oxide flakes, the thickness of the nanosheets is 24 nm, and the particle size is 0.06 μm. The other steps and parameters are the same as those in Embodiment 1.
specific Embodiment approach 3
[0025] Specific embodiment three: the difference between this embodiment and specific embodiment one or two is: the concentration of graphene in the described one based on flower-like zinc oxide@ferrocene functionalized three-dimensional graphene composite is 19mg / mL~ 22mg / mL. And freeze-dried at -40°C for 24 hours in a freeze dryer. Other steps and parameters are the same as those in Embodiment 1 or 2.
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