Durable styling compositions and the uses thereof
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examples 1-96
[0086]Eighty-eight examples of the invention are prepared having a PVM / MA copolymer and polyimide-1 (Aquaflex® XL-30, 30% active); (Table 3, and Tables 4-11). For each choice of PVM / MA copolymer, 8 formulas are made. An acidic polymer solution with a pH of about 2 is produced after adding the PVM / MA copolymer to water. Under these very low pH conditions a complex results when polyimide-1 was added. In order to obtain a smooth solution of both polymers, the following procedure is followed: The PVM / MA copolymer is dissolved with about 40% of the water in a first vessel, after which the pH is adjusted to 3.5 using sodium hydroxide. In a second vessel the remaining water is mixed with the polyimide-1, and then this solution is added to contents of the first vessel. After mixing well the preservative (if any) is added the blended to yield a translucent, viscous polymeric solution. The selected preservative is a blend of phenoxyethanol and caprylyl glycol. The pH of the durable styling co...
example 97-192
[0087]Concentrated versions of Examples 1-96 are made to 22.5% (w / w) total solids (Table 12). The choice of PVM / MA copolymer follows the same sequence as in the examples above. First, tetrasodium ethylenediaminetetraacetic acid EDTA Na4 is added to the water with mixing until uniform. Then, the PVM / MA copolymer is dispersed into the water with good mixing. The pH is adjusted with 50% NaOH solution to pH of about 4.5 before adding the polyimide-1, which is mixed-in until uniform. The caprylyl glycol and phenoxyethanol / caprylyl glycol are added individually, mixing until uniform. Once the mixture is uniform, the pH was adjusted to 7.1±0.2 with NaOH solution. Example 192 with Gantrez® S-97 was reduced to practice.
TABLE 12Concentrated formulations of Example 97-192additioningredientlevel (% w / w)water45.85EDTA Na4 (Versene ® 100, Dow)0.75PVM / MA copolymer15.00polyimide-1 (Aquaflex ® XL-30, ASI)25.00caprylyl glycol1.90phenoxyethanol and caprylyl glycol1.50(Optiphen ®, ASI)NaOH (50% solutio...
example 193-288
[0088]Concentrated versions for the formulation of Examples 1-96 are prepared at 30% (w / w) solids (Table 13). The choice of PVM / MA copolymer follows the same sequence as in the examples above. EDTA Na4 is added at 1.00% (w / w) as a chelating agent for metal ions. The pH of this concentrate is adjusted to 7.9±0.2 by the addition of 11.1 grams of sodium hydroxide (50% solution) for every 100 grams of concentrate. Example 288 with Gantrez® S-97 was reduced to practice.
TABLE 13Concentrated formulations of Examples 193-288additioningredientlevel (% w / w)water38.20EDTA Na4 (Versene ® 100, Dow)1.00PVM / MA copolymer20.00polyimide-1 (Aquaflex ® XL-30, ASI)33.30phenoxyethanol and caprylyl glycol7.50(Optiphen ®, ASI)total100.00
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