39 results about "Deer musk" patented technology

The invention discloses an ambergris-amber flavor essence, which is characterized by comprising the following components in part by weight: 16 parts of vanilline, 4 parts of piperonal, 3 parts of sage clary oil, 0.6 part of viverra civetta schreber, 2 parts of storax balm, 10 parts of vanilla bean extract, 20 parts of santal oil, 6 parts of patchouli oil, 0.2 part of rose absolute, 2 parts of methylionone, 1 part of bitter orange flower oil, 30 parts of bergamot oil, 13 parts of coumarin, 5 parts of ambergris, 16 parts of musk xylene, 15 parts of benzoin balm, 1.6 parts of frostweed extract, 16 parts of coriander seed oil, 10 parts of vetiver oil, 3 parts of jasminum grandiflorum absolute, 6 parts of fleur-de-lis extract, 3 parts of lavender absolute and 10 parts of lemon oil. The ambergris-amber flavor essence of the prescription is suitable for flavoring products such as white cream, latex, shampoo and the like, has no defect of discoloring, and has the advantages of pure and rich flavor, strong persistence, extremely little dosage and the like.

The invention discloses a chrysanthemum essence for hand cream, which is characterized by comprising the following components by weight percent: 2 parts of vetiver oil, 2 parts of cinnamon bark oil, 14 parts of sandal oil, 28 parts of alpha-terpineol, 8 parts of jasmine fragrance base, 36 parts of geranium oil, 20 parts of ylang ylang oil, 30 parts of hydroxycitronellal, 20 parts of lavender oil, 12 parts of bergamot oil, 8 parts of isoeugenol, 2 parts of iris resin, 2 parts of musk ketone, 8 parts of Peru musk, 16 parts of heliotropin and 2 parts of vanillin. The chrysanthemum essence for the hand cream is suitable for fragrance products of white cream, skin milk, fragrant molasses and the like, has no defect of discoloration, and has the advantages of pure and rich fragrance, strong durability, extremely less using quantity and the like.

The invention relates to a method which can stably detect the concentration of synthetic musk in breast milk, and the purpose of measuring the concentration of the synthetic musk in the breast milk is achieved through the combined method of the gel chromatographic column chemical pretreatment method and the gas chromatography-mass spectroscopy. The method belongs to the technical field of physical and chemical analysis and measurement of organic chemical materials. The pretreatment process of the breast milk in the method of the invention comprises liquid-liquid extraction and the step of passing through the gel chromatographic column, the solution after the concentration by eluting solution is processed by passing through a small silica gel column and finally enters a gas chromatograph-mass spectrograph (GC-MS) for carrying out the detection, thereby obtaining a mass spectrum curve diagram containing various synthetic musk in the breast milk sample and then utilizing the specific formula for calculating the content of the musk contained in the breast milk. The method of the invention is an effective measurement method which is stable and has higher accuracy.

The invention provides a method for determining the content of musk ketone in artificial musk, and the method comprises the following steps: step 1, preparing the solution of an artificial musk test sample and musk ketone reference solutions; step 2, by using a capillary gas chromatography, assaying the reference solutions to acquire a standard curve; and step 3, determining the content of musk ketone in the artificial musk test sample according to the standard curve. The method for determining the content of musk ketone in artificial musk of the present invention is simple and reliable, thus being suitable for industrial mass production.

The invention relates to a compound feed for young forest musk deer and a processing method thereof, and belongs to the technical field of processing methods. The compound feed for young forest musk deer comprises the following raw materials in parts by weight: 45-60 parts of corn, 12-30 parts of oat, 20-35 parts of Chenopodium quinoa willd, 8-12 parts of rye, 10-15 parts of soybean, 5-10 parts of green beans, 8-14 parts of chickpea, 15-22 parts of bran, 4-10 parts of bean pulp, 4-10 parts of cottonseed meal, 5-10 parts of peanut meal, 4-8 parts of greaves, 5-12 parts of bone meal, and 3-5 parts of egg shells. The compound feed for young forest musk deer is combined with green grasses for feeding, not only can effectively supplement nutrient elements required by the growing of the forest musk deer, but also can promote quick growing of the forest musk deer, also can effectively enhance the immunity of the forest musk deer and reduce the occurrences of diseases, and further can effectively promote musk secretion in a later period.

The invention discloses a method for identifying natural musk and muskone. The method comprises the following step: with hexacosanoic acid and octacosanoic acid as reference substances, performing qualitative identification by adopting an ultrahigh performance bonded-phase chromatography-tandem mass spectrometry method. The method disclosed by the invention is used for identifying the natural musk and the muskone; a sample is simple in pretreatment, and rapid, accurate, and environmentally friendly in detection.

The invention discloses a method for efficient synthesis of musk tibetene from 1, 2, 3-trimethylbenzene. The method includes: firstly letting 1, 2, 3-trimethylbenzene undergo Friedel-Crafts alkylation reaction to generate 5-tertbutyl-1, 2, 3-trimethylbenzene, then under catalysis of Lewis acid, making the 5-tertbutyl-1, 2, 3-trimethylbenzene react with nitric acid to generate musk tibetene, then carrying out follow-up technological treatment by subjecting the reaction mixture to dilution, neutralization and filtration, and then conducting separation by recrystallization, thus obtaining a pure product. The synthetic method provided by the invention is simple and efficient, has low requirement for raw materials, and has no need for ultra-high purity 1, 2, 3-trimethylbenzene. The requirements for reaction conditions are low, and by means of simple follow-up treatment steps, the high purity musk tibetene can be obtained. In addition, compared with the prior art, the method provided by the invention causes much lower environmental pollution.

The invention provides a forest musk deer feed premixing agent formula and a use method thereof. The problems that the reproduction rate of the forest musk deer is low at present and the forest musk deer cannot be bred on a large scale and is scarce because of various limits in other artificial feeding methods are solved. The premixing agent formula is prepared from vitamin, folic acid, copper, iodine, egg cyanamide and the like; the forest musk deer is fed with the premixing agent, so that the forest musk deer can develop healthily, the reproduction rate and the farrowing rate of the forest musk deer are increased, the yield of musk is increased and the disease resistance is improved.

The invention discloses a method for extracting musk from a living musk rat. The method comprises the following steps: massaging the musk rat, catching the musk rat, enabling the musk rat to be excited and extracting musk. The invention provides the method for extracting musk from the living musk rat sweetly. Compared with methods of hunting musk rats for extracting musk and extracting musk from a living musk rat, the method provided by the invention has the advantages that the musk yield of the musk rat is enabled to be increased by 50 percent, and the annual musk yield is increased to 10 to 15 grams from the 5 to 6 gram before.

The invention belongs to the technical field of moschus berezovskii breeding and discloses a secondary musk secretion method for young and middle-aged moschus berezovskii. 300 microgrammes of an LHRH-A3 medicine is administrated for the young and middle-aged moschus berezovskii through intramuscular injection, and 100 microgrammes of the LHRH-A3 medicine is administrated through hypodermic injection. A source hormone is used to stimulate gonad axis through positive feedback to release gonadal hormone, the male moschus berezovskii secretes musk for the second time, so that the yield of the musk is increased under the condition of the limited number of cultured stocks, and the economic benefit of the moschus berezovskii is greatly improved; the hypophysis is induced to secrete the positive feedback hormone by increasing the dose of a hypothalamus related hormone receptor, the sex hormone is promoted to secrete the musk, and the theoretical support is provided for the musk secretion mechanism. The male moschus berezovskii secretes the musk for the second time, so that the survival quality of the endangered animal moschus berezovskii is helped improved under the captive conditions, the technical support is provided for improving the yield of the traditional Chinese animal medicine musk, and the industrial development of artificial breeding of the moschus berezovskii is also promoted.

The invention discloses a rose-musk essence, which is characterized in that: the rose-musk essence comprises the following compositions in percentage by weight: 7.5 to 8 percent of musk xylene, 5.5 to 6.0 percent of eugenol, 12 to 14 percent of galaxolide musk, 8.0 to 8.5 percent of geraniol, 5.0 to 5.5 percent of tonalid, 4.0 to 5.0 percent of citronellol, 2.8 to 3.2 percent of methyl cedryl ketone, 6.5 to 7.0 percent of 3,3-dimethylcyclohexyl methyl ketone, 9.0 to 11.0 percent of lilial, 5.0 to 5.4 percent of phenethyl alcohol, 2.8 to 3.0 percent of geranylacetone, 0.8 to 1.0 percent of capryl alcohol, 3.8 to 4.4 percent of coumarin, 20.0 to 24.0 percent of iso-longitolanone and 16.0 to 18.0 percent of heliotropin. The rose-musk essence is suitable for fragrant products such as white cream, lotion, fragrant molasses and the like, does not have the defect of color change, and has the advantages of pure and rich fragrance, strong persistance, low consumption and the like.

The present invention relates to compounds of Formula (I), wherein the dotted line represents a carbon-carbon single or double bond and R represents a hydrogen atom or a methyl group; which are useful perfuming ingredients to impart odor notes of the musky-earthy and woody, aromatic-fresh type.

The present invention discloses one kind of Chinese medicine composition for treating cardiac vascular diseases and its preparation process. The Chinese medicine composition is prepared with red sage, notoginseng and musk or muskone as the material medicines. The preparation process includes the following steps: 1. extracting red sage and notoginseng with water or alcohol to obtain extracted solution; 2. clarifying the extracted solution; 3. ultrafiltering the extracted solution; and 4. concentrating the filtrate to obtain extractum, and mixing the extractum with musk or muskone. The Chinese medicine composition may be prepared into different preparations, preferably dripping pill.

A lavender aroma type automobile foot pad is composed of a traditional Chinese medicine blanket blank layer, an anion gluing layer and an anti-skid layer. Traditional Chinese medicine particle containing cavities and active mineral substance particle containing cavities are sequentially formed between the traditional Chinese medicine blanket blank layer and the anti-skid layer at intervals. The traditional Chinese medicine particle containing cavities and the active mineral substance particle containing cavities are a plurality of strip-shaped cavities distributed in a pedal part and side wing parts at equal intervals. Traditional Chinese medicine particles are contained in the traditional Chinese medicine particle containing cavities and comprise, by weight, 70-80 parts of rhamnus crenata, 3-5 parts of the root of bidentate achyranthes, 1-3 parts of common bluebeard herb, 15-20 parts of cyrtomium fortunei, 20-25 parts of lavender, 3-5 parts of anemone hupehensis, 15-25 parts of elm bark, 4-6 parts of agilawood, 20-25 parts of camphorwood, 3-5 parts of storax, 1-3 parts of musk, 1-3 parts of mint, 1-3 parts of astragalus membranaceus, 1-3 parts of mother chrysanthemum, 1.5-2.5 parts of sweet marjoram and 1.5-2 parts of sandalwood. The lavender aroma type automobile foot pad is high in safety performance and not only can effectively repel mosquitoes but also can release anions; meanwhile, the odor is fragrant, the character is moderate, freshness and spirit invigoration are achieved, and high application value is achieved.

The invention relates to a feeding method for musk in a musk extraction process. The feeding method comprising the steps of uniformly mixing the musk and other solid particles, sub-packaging into bagsand bundling openings through fine lines is adopted, the musk is not agglomerated in an extraction process and is in sufficient contact with an extraction medium, the extraction rate is improved andthe problem that the content of extracted muskone is low is solved, so that the quality of a preparation is improved and relatively good technical effects are obtained.

The invention provides a three-dimensional reconstruction method of a forest musk deer gland tissue and aims to solves the technical problems that a forest musk deer musk secretion mechanism cannot bedeveloped in the aspects of tissue and cellular morphological structure and the yield increase of musk cannot be further deeply researched in the prior art. The method comprises the steps of sampling, slicing, dyeing, scanning, three-dimensional reconstruction and the like of the forest musk deer gland tissue. According to the three-dimensional reconstruction method of the forest musk deer glandtissue, tissue slice dyeing is used for achieving in-vitro visualization of the musk gland tissue, and a good application effect is achieved; the physiological structure of the forest musk deer glandtissue is researched by the in-vitro visualization method of the forest musk deer gland tissue, and the three-dimensional in-vitro structure of the forest musk deer gland tissue is shown for the firsttime, so that the morphological structure content of the forest musk deer gland tissue is enriched, meanwhile, a morphological basis is provided for deeply researching the musk secretion reaction ofthe forest musk deer and improving the musk yield.

A natural mosquito-repellent plant and active mineral combined front-wall sound-insulating pad for an automobile comprises a traditional Chinese medicine blanket blank layer, an anion adhesion layer and an anti-skidding layer, wherein traditional Chinese medicine particle accommodating cavities and active mineral particle accommodating cavities are further sequentially arranged between the traditional Chinese medicine blanket blank layer and the anti-skidding layer in a space manner, and are a plurality of strip-shaped cavities equidistantly distributed at a foot part and side wing parts; traditional Chinese medicine particles are accommodated in the traditional Chinese medicine particle accommodating cavities, and contain 70-80 parts of Chinese wingleaf pricklyash fruits, 3-5 parts of common clubmoss herbs, 1-3 parts of liquorice, 20-25 parts of semen torreya, 15-20 parts of lavender, 3-5 parts of Japanese anemones, 3-5 parts of hupeh anemone herbs, 15-25 parts of elm bark, 4-6 parts of Chinese eaglewood, 20-25 parts of camphorwood, 3-5 parts of styrax, 1-3 parts of musk, 1-3 parts of mint, 1-3 parts of flos rhododendri mollis, 1.5-2.5 parts of sweet marjoram and 1.5-2 parts of lignum Santali albi. The sound-insulating pad has relatively high safety performance, not only can effectively repel mosquitos and other insects, but also can release anions, is aromatic in smell, mild in nature, fresh and refreshing, and has broad application value.

The present invention discloses one kind of Chinese medicine composition for treating cardiac vascular diseases and its preparation process. The Chinese medicine composition is prepared with red sage, notoginseng and musk or muskone as the material medicines. The preparation process includes the following steps: 1. extracting red sage and notoginseng with water or alcohol to obtain extracted solution; 2. clarifying the extracted solution; 3. ultrafiltering the extracted solution; and 4. concentrating the filtrate to obtain extractum, and mixing the extractum with musk or muskone. The Chinese medicine composition may be prepared into different preparations, preferably dripping pill.

The invention discloses a method for preparing musk ketone efficiently and mildly. The method comprises the following steps: crushing musk, sieving musk, soaking musk by using ethanol, performing reflux extraction by using ethanol, and performing reflux extraction by using water to obtain a filtrate; soaking a filter residue by using hot water, and performing hot-pressing distillation extraction to obtain a hot-pressed extract; concentrating the hot-pressed extract and the filtrate, centrifuging, washing, and dissolving in distilled water to obtain a dissolved solution; adjusting the pH of the dissolved solution, filtering by using a ceramic membrane, circularly washing, adding pure water for dissolving, decolorizing, filtering, and performing spray drying to obtain the musk ketone. By the method, the purity of the musk ketone can be increased, and reaches above 99%; the preparation process is simple, and easy to operate; a treatment condition is mild, so that the musk ketone is not affected; the extracting effect is good, more than 99% of the musk ketone in the musk can be extracted; the method has the advantages of high efficiency, rapidness, achievement of high purity, and the like.

The invention relates to an identification method for diphenhydramine hydrochloride and procaine hydrochloride in a musk blood circulation promoting and blood stasis removing ointment. The method includes the following steps: firstly dissolving the ointment through diethyl ether; then adding water for dissolving; extracting the diphenhydramine hydrochloride and the procaine hydrochloride in the ointment; standing, skimming, washing the water solution through the diethyl ether, and filtering through a piece of dry filter paper; measuring a filtrate through the high performance liquid chromatography. The identification method is excellent in reproducibility, strong in specificity, avoids interference in negative control, can be used for one-time simultaneous qualitative identification for the diphenhydramine hydrochloride and the procaine hydrochloride in the musk blood circulation promoting and blood stasis removing ointment, and is applicable to quality control of the musk blood circulation promoting and blood stasis removing ointment.

Argy wormwood leaf traditional Chinese medicine mosquito-repellent incense belongs to the technical field of a mosquito-repellent product. The mosquito-repellent incense comprises, 30-50 parts of waste paper fiber, 5-15 parts of argy wormwood leaves, 1-5 parts of flos genkwa, 15-25 parts of elm barks, 1-3 parts of sandalwood, 1-3 parts of mint, 0.5-1.5 parts of musk, 25-40 parts of mosquito-repellent vanilla, 5-12 parts Sichuan chinaberry barks, 3-8 parts of Aztec marigold, 4-8 parts of mandarin orange peel, 5-20 parts of muntiacus reevesi micrurus, and 8-15 parts of clove. The mosquito-repellent incense has an effective mosquito-repellent effect for a long time and is low in raw material cost. The mosquito-repellent incense produces extremely less harmful substances during combustion andis non-toxic or harmless to the human body. The mosquito-repellent incense has a certain inhibition and killing effect on pathogens including staphylococcus aureus and dysentery bacillus.

The present invention relates to a detection method for a sare thirteen-flavored penniao preparation provided by the present invention. On the basis of the original standard, the present invention adds the identification of chebula, woody, nutmeg and musk of precious medicinal materials, and adds the inspection of aconitine in the iron club, which further ensures the safety, uniformity, effectiveness and controllable quality of the product.

The invention relates to a method for determining the content of panax pseudoginseng in musk ointment for promoting blood circulation by removing blood stasis. The method comprises the steps of dissolving ointment with diethyl ether firstly, then adding water for dissolving, extracting Rg1, Rb1 and R1, standing, separating liquid, washing water liquid with the diethyl ether, filtering with dry filter paper and determining the filtrate by using a high performance liquid chromatography. The determination method has relatively high accuracy and precision degree, easiness and convenience for operation, strong specificity and durability and can be used for quality control of the musk ointment for promoting the blood circulation by removing the blood stasis.

The invention discloses a method for detecting synthetic musk. Muscone, 4-methyl-cyclopentadecanon, musk lactone, dehydrogenated musk lactone and C18H2803 of synthetic musk in a medicine are qualitatively detected, so as to judge whether the medical synthetic musk conforming to the regulations of the pharmacopeia is used in the medicine. Through the method, the safety and effectiveness of the medicine can be judged accurately, and the medicine quality is controlled more comprehensively.

The invention relates to a method for purifying phosphorylated eledoisin, and belongs to the technical field of chemical purification. The phosphorylated eledoisin has very strong antihypertensive activity, and a chemosynthetic crude product of the phosphorylated eledoisin is difficult to purify in quantity, so that the application of the phosphorylated eledoisin is limited. The purification and preparation of the chemosynthetic phosphorylated eledoisin are realized by dint of technologies, namely vacuum filtration and the like, through three key steps of sample loading, cleaning and elution by utilizing a principle that titanium dioxide and the phosphorylated eledoisin generate higher Lewis acid-base effect in an acid environment and the Lewis acid-base effect disappears in an alkaline environment and adopting an independently researched phosphorylated polypeptide purification device (an application number: 201420158316.9). The method disclosed by the invention is easy and convenient to operate, economy and high-efficiency, and provides an effective method for the purification of the phosphorylated eledoisin, thereby promoting the application of the phosphorylated eledoisin in the fields of medicines and the like.

The present invention relates to the technical field of medicinal effective ingredients, in particular to a thin layer identification method for effective ingredients of Panax notoginseng in musk blood circulation promoting and blood stasis removing paste. The method comprises: a thin layer identification method for atropine sulfate and a thin layer identification method for diphenhydramine hydrochloride. Through characteristics of each pharmaceutical ingredient in the musk blood circulation promoting and blood stasis removing paste, and based on thin layer identification characteristics of the effective ingredients of the Panax notoginseng, the method provides a suitable extraction preparation process and required preparations, thereby being able to separate and extract the ingredients tobe measured from the effective pharmaceutical ingredients of the musk blood circulation promoting and blood stasis removing paste to complete the thin layer identification measurement; and the methodsolves the problem that the musk blood circulation promoting and blood stasis removing paste is emplastrum in combination of Chinese and western medication, that sample coating is carried out at a high temperature, that all effective substances are in colloid, and that more accurate results can not be obtained caused by difficulties to separately extract the effective ingredients from the Panax notoginseng through the existing thin layer identification method in analysis of the effective pharmaceutical ingredients.

The invention provides a quantitative analysis method for plasma concentration of musk ketone in artificial musk. The quantitative analysis method comprises the following steps of: adding acetonitrile and an internal standard working solution into plasma of a rat lavaged by the artificial musk, mixing, vortexing, centrifuging, taking supernatant and filling in a headspace sampling bottle of a headspace sampler to test and also adding 1-5 percent by weight of NaCl aqueous solution into the headspace sampling bottle, wherein the internal standard solution is alcoholic solution of cyclohexanone or normal hexane; and determining by using a gas chromatography-mass spectrometry method. According to the quantitative analysis method, the headspace sampling gas chromatography-mass spectrometry method is adopted, the method for precipitating protein by using the acetonitrile is used as a biological sample pretreatment method, and the determination is performed under proper temperature programming conditions and at proper headspace balance temperature and proper headspace balance time. The determination method has high specificity and high sensitivity, is quick and convenient to determine, can greatly simplify an experimental process and is suitable for pharmacokinetic study.