Method for manufacturing selenium-rich fucoidin
A polysaccharide and selenium-enriched technology, applied in animal feed, animal feed, additional food elements, etc., can solve problems such as potential safety hazards, and achieve the effect of avoiding harm and controlling selenium content
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Embodiment approach 1
[0015] Take 30g of edible grade fucoidan sulfate, make it into 10% aqueous solution, add Na 2 SeO 3 20g, HCl15ml, add selenizing agent at a constant temperature of 80°C, react for 24 hours, centrifuge to remove a small amount of insoluble matter, use a membrane device with a molecular weight cut-off of 20,000 for ultrafiltration, and check the inorganic selenium in the effluent at any time until it is confirmed that it does not exist As far as inorganic selenium is concerned, selenium-enriched fucoidan with a selenium content of 0.45% is obtained.
Embodiment approach 2
[0017] Take 30g of edible grade fucoidan sulfate, make it into 10% aqueous solution, add Na 2 SeO 3 20g, HNO 3 15ml, add selenizing agent at a constant temperature of 80°C, react for 24 hours, centrifuge to remove a small amount of insoluble matter, use a membrane device with a molecular weight cut-off of 20,000 for ultrafiltration, and check the inorganic selenium in the effluent at any time until it is confirmed that there is no inorganic selenium So far, the selenium-enriched fucoidan with a selenium content of 0.36% has been obtained.
Embodiment approach 3
[0019] Take 30g of edible grade fucoidan sulfate, make it into 10% aqueous solution, add Na 2 SeO 3 15g, HCl and 15ml of acetic acid, add selenizing agent at a constant temperature of 80°C, react for 24 hours, centrifuge to remove a small amount of insoluble matter, use a membrane device with a molecular weight cut-off of 20,000 for ultrafiltration, and detect the inorganic selenium in the effluent at any time until Until it is confirmed that there is no inorganic selenium, the selenium-enriched fucoidan with a selenium content of 0.45% is obtained.
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