Process for carrying out pretreatment on waste oil
A waste oil and pretreatment technology, which is applied in the direction of fat oil/fat refining and fat production, can solve the problems of unstable source, difficult unsaponifiable components, increasing the number and content of waste oil unsaponifiable components, etc., to improve oil Quality, reduction of coking, good raw material quality assurance effect
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Embodiment 1
[0016] Embodiment 1: A waste oil pretreatment process of the present invention includes the following steps: adding waste oil into the pressure-resistant reactor of the reaction device, gradually turning on the steam under stirring and raising the temperature to 80°C, and then adding 40% of the total weight of waste oil Add the following decomposition agents in order: 2.5% concentrated sulfuric acid, 1.5% phosphoric acid, 1.5% sulfoxylyl fatty acid, the amount of the above decomposition agents is the weight percentage calculated based on the total weight of waste oil, continue Raise the temperature to 130°C, adjust the steam pressure and supply, and keep the temperature and pressure stable. After that, take a sample of the reaction material every hour to measure the acid value of the material. When the acid value of the reaction material rises to 160mgKOH / g in about 4 to 6 hours, turn off the steam. Stop heating; when the temperature drops to 95°C, turn off the stirring, and af...
Embodiment 2
[0017] Embodiment 2: A waste oil pretreatment process of the present invention includes the following steps: adding waste oil into the pressure-resistant reactor of the reaction device, gradually turning on the steam under stirring state and raising the temperature to 85°C, and then adding 30% of the total weight of waste oil Add the following decomposition agents in order: 1.5% concentrated sulfuric acid, 1.5% phosphoric acid, 1.5% sulfoxylyl fatty acid, the amount of the above decomposition agents is the weight percentage calculated based on the total weight of waste oil, continue Raise the temperature to 120°C to 140°C, adjust the steam pressure and supply rate, and keep the temperature and pressure stable. After that, the reaction material is sampled every hour to measure the acid value of the material. When the acid value of the reaction material rises to 140mgKOH / g in about 4 to 6 hours, Turn off the steam and stop heating; when the temperature drops to 95°C, turn off the...
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