Fingerprint spectrum detection method for postnatal Gongtai granules
A Gongtai granule and detection method technology, which is applied in the direction of measuring devices, instruments, scientific instruments, etc., can solve the problems of inability to fully characterize the quality of hot shower clear, and achieve the effect of ensuring accuracy and correctness
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[0022] In order to facilitate the understanding of those skilled in the art, the present invention will be further described below in conjunction with the embodiments and accompanying drawings.
[0023] 1. Instruments and reagents
[0024] 1.1 Instrument
[0025] EL1600 high performance liquid chromatograph and its original workstation.
[0026] 1.2 Reagent
[0027] The reference substance of ginsenoside Rg1 was provided by China Institute for the Control of Pharmaceutical and Biological Products; acetonitrile was chromatographically pure; postpartum Gongtai granules were provided by Hefei Jinyue Pharmaceutical Co., Ltd., and the batch numbers were 120101, 120102, 120201, 120301, 120501, 120502, 120601, 120602, 120801, 120802.
[0028] 2. Methods and Results
[0029] 2.1 Chromatographic conditions and system suitability
[0030] Use octadecylsilane bonded silica gel as filler (250×4.6mm, 5μm); use acetonitrile as mobile phase A and water as mobile phase B, and carry out g...
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