A kind of preparation method of traditional Chinese medicine preparation snake gallbladder tangerine peel oral liquid

A technology of snake gallbladder tangerine peel and oral liquid, applied in the field of medicine, can solve the problems of insufficient extraction of hesperidin and the like

Active Publication Date: 2016-01-13
JIANGXI JIMINKEXIN PHARMA +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The present invention aims to provide a new preparation method of Shedan tangerine peel oral liquid, solve the problem of insufficient extraction of hesperidin, and improve the transfer rate of active ingredients of medicinal materials
At the same time, a certain concentration of ethanol is used as an extraction solvent to extract the active ingredient of hesperidin in the medicinal material of tangerine peel, and a certain concentration of alkali solution is added to the clear ointment to adjust the pH to a certain range, which not only solves the problem of the solubility of hesperidin, but also solves the problem of this variety. Clarity issues

Method used

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  • A kind of preparation method of traditional Chinese medicine preparation snake gallbladder tangerine peel oral liquid

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0050] The dried tangerine peel was extracted with 4 times the amount of 50% ethanol solution at reflux once for 0.5 hours and filtered. The filtrate was decompressed to recover ethanol, and concentrated to no alcohol smell. Adjust the pH of alkaline water to 12.0 for use. Measure 300 ml of purified water, add the prepared tangerine peel liquid to the above purified water, add acid water to adjust the pH to 5.8, and sink. Take the supernatant, add 50ml of snake bile, almond water, 30ml of ginger water, 240g of sucrose and 0.5g of hydroxybenzene diester, dissolve, filter, add water to a constant volume of 1000ml, 10ml / bottle filling, sterilization, packaging, that is Got.

Embodiment 2

[0052] The dried tangerine peel was extracted twice with 6 times the amount of 50% ethanol solution and refluxed for 1 hour each time, filtered, and the filtrate was combined. The filtrate was decompressed to recover ethanol, and concentrated to no alcohol smell. Adjust the pH of alkaline water to 12.0 for use. Measure 300 ml of purified water, add the prepared tangerine peel liquid to the above purified water, add acid water to adjust the pH to 5.8, and sink. Take the supernatant, add 50ml of snake bile, almond water, 30ml of ginger water, 240g of sucrose and 0.5g of hydroxybenzene diester, dissolve, filter, add water to a constant volume of 1000ml, 10ml / bottle filling, sterilization, packaging, that is Got. Example 3

Embodiment 3

[0053] The dried tangerine peel was extracted three times with 8 times the amount of 50% ethanol solution under reflux for 1.5 hours each time, filtered, and the filtrate was combined. The filtrate was decompressed to recover ethanol, and concentrated to no alcohol smell. Adjust the pH of alkaline water to 12.0 for use. Measure 300 ml of purified water, add the prepared tangerine peel liquid to the above purified water, add acid water to adjust the pH to 5.8, and sink. Take the supernatant, add 50ml of snake bile, almond water, 30ml of ginger water, 240g of sucrose and 0.5g of hydroxybenzene diester, dissolve, filter, add water to a constant volume of 1000ml, 10ml / bottle filling, sterilization, packaging, that is Got.

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Abstract

The invention relates to a preparation method of a Chinese herba preparation and particularly relates to a new preparation method of snake gall-dried orange peel oral liquid, belonging to the technical field of medicines. The preparation method of the snake gall-dried orange peel oral liquid comprises the following steps of: extracting dried orange peel with ethanol and removing ethanol out of the extracting liquid; then, adding alkaline water so that the extracting liquid becomes alkaline; adding water to adjust pH to 5-6 and separating out precipitates; filtering; and adding snake gall and medicinal auxiliaries to the filtrate so as to finally obtain the snake gall-dried orange peel oral liquid.

Description

Technical field [0001] The invention relates to a preparation method of traditional Chinese medicine preparations, in particular to a new preparation method of snake gall and tangerine peel oral liquid, belonging to the technical field of medicine. Background technique [0002] Shedan Chenpi oral liquid has the effects of smoothing Qi, eliminating phlegm, expelling wind and strengthening stomach. The dried tangerine peel in the recipe is derived from the dried and mature peel of the rutaceae plant Citrusreticulata Blanco and its cultivars. It has the functions of regulating qi and strengthening the spleen, drying dampness and reducing phlegm. It is used for abdominal distension, poor appetite, vomiting, cough and phlegm. medicine. Shedan Chenpi oral liquid is clinically used for wind-cold cough, phlegm and hiccups. The usage and dosage is oral, 10ml each time, 2-3 times a day. The dried tangerine peel hesperidin in the prescription is a flavonoid compound, which is almost inso...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K36/752A61K36/9068A61K9/08A61P11/10A61P1/14A61P11/14A61K35/583A61K31/7048
Inventor 易航文万江惠刚
Owner JIANGXI JIMINKEXIN PHARMA
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