Extraction method for persimmon tannin
An extraction method and technology of persimmon, applied in the field of extraction of persimmon tannin, to achieve the effect of inhibiting Streptococcus mutans
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Embodiment 1
[0016] 1) Peel and crush the persimmons, add 70v% ethanol 10 times the weight of the persimmons, extract at 60°C for 1 hour, combine the extracts, filter, and take the filtrate for later use;
[0017] 2) Concentrate the filtrate, add 95v% ethanol, the amount of ethanol added is 2 times of the concentrated solution, leave it overnight, centrifuge, and take the supernatant;
[0018] 3) Pass the supernatant through AB-8 macroporous resin, wash the column with water until it is colorless, then elute with ethanol, and collect the ethanol eluate;
[0019] 4) Concentrate the ethanol eluent to recover the solvent to obtain the extract, add water to dissolve, the amount of water added is 3 times the weight of the extract, filter, take the filtrate and pass it through a hollow fiber membrane with a molecular weight cut-off of 450-600, and collect the retentate for later use ;
[0020] 5) passing the retentate through a hollow fiber membrane with a molecular weight cut-off of 14,000-15,...
Embodiment 2
[0022] 1) Peel and crush the persimmons, add 80v% ethanol 20 times the weight of the persimmons, extract 3 times at 80° C. for 3 hours each time, combine the extracts, filter, and take the filtrate for later use;
[0023] 2) Concentrate the filtrate, add 95v% ethanol, the amount of ethanol is 4 times that of the concentrated solution, leave it overnight, centrifuge, and take the supernatant;
[0024] 3) Pass the supernatant through AB-8 macroporous resin, wash the column with water until it is colorless, then elute with ethanol, and collect the ethanol eluate;
[0025] 4) Concentrate the ethanol eluate to recover the solvent to obtain the extract, add water to dissolve it, the amount of water added is 5 times the weight of the extract, filter, take the filtrate and pass it through a hollow fiber membrane with a molecular weight cut-off of 450-600, and collect the retentate for later use ;
[0026] 5) passing the retentate through a hollow fiber membrane with a molecular weigh...
Embodiment 3
[0028] 1) Peel and crush the persimmons, add 75v% ethanol 15 times the weight of the persimmons, extract twice at 70°C for 2 hours each time, combine the extracts, filter, and take the filtrate for later use;
[0029] 2) Concentrate the filtrate, add 95v% ethanol, the amount of ethanol added is 3 times of the concentrated solution, leave it overnight, centrifuge, and take the supernatant;
[0030] 3) Pass the supernatant through AB-8 macroporous resin, wash the column with water until it is colorless, then elute with ethanol, and collect the ethanol eluate;
[0031] 4) Concentrate the ethanol eluate to recover the solvent to obtain the extract, add water to dissolve, the amount of water added is 4 times the weight of the extract, filter, take the filtrate and pass it through a hollow fiber membrane with a molecular weight cut-off of 450-600, and collect the retentate for later use ;
[0032] 5) passing the retentate through a hollow fiber membrane with a molecular weight cut-...
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