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Production method of zno nano material fabric and zno nano material fabric

A technology of nanomaterials and production methods, applied in the field of nanomaterials, can solve the problems of low yield, uneven distribution of nano-ZnO layers, difficult operation, etc., and achieves the effect of cost, high cost of raw materials, and complex preparation process.

Active Publication Date: 2018-10-09
NANTONG TEXTILE & SILK IND TECH RES INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the most important is the two-step growth method ZnO surface, but this method is difficult to operate, the yield is low, and the nano-ZnO layer on the fabric is unevenly distributed

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Production method of zno nano material fabric and zno nano material fabric
  • Production method of zno nano material fabric and zno nano material fabric
  • Production method of zno nano material fabric and zno nano material fabric

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0049] Step 1: PDMS modified clean cotton cloth.

[0050] In one embodiment, this step can be specifically performed as follows: First cut several pieces of the fabric according to the size of 3×3cm, put them in a beaker, pass through deionized water once, and ultrasonicate with absolute ethanol for 5 minutes, and put it in an oven at 80°C after ultrasonication Dry and cool for later use. Dissolve 3ml of PDMS in 500ml of tetrahydrofuran, continue to stir for 1 hour under the action of a magnetic rotor, add to the solution, wash with water and absolute ethanol in sequence, and dry the spare fabric, soak for 2 minutes; take it out and dry it at 80°C.

[0051] Step 2: the oil bath method is used to prepare the fabric with the surface of the nanometer ZnO particle layer.

[0052] In one embodiment, this step can specifically be performed as follows: 2g zinc acetate, 1.5g vitamin C are dissolved in 100ml deionized water and stirred evenly under the action of a magnetic rotor, then...

Embodiment 2

[0055] Step 1: PDMS modified clean cotton cloth.

[0056] In one embodiment, this step can be specifically performed as follows: First cut several pieces of the fabric according to the size of 3×3cm, put them in a beaker, pass through deionized water once, and ultrasonicate with absolute ethanol for 5 minutes, and put it in an oven at 80°C after ultrasonication Dry and cool for later use. Dissolve 5ml of PDMS in 500ml of tetrahydrofuran, continue to stir for 1 hour under the action of a magnetic rotor, add to the solution, wash with water and absolute ethanol in sequence, and dry the spare fabric, soak for 2 minutes; take it out and dry it at 100°C.

[0057] Step 2: the oil bath method is used to prepare the fabric with the surface of the nanometer ZnO particle layer.

[0058] In one embodiment, this step can be specifically performed as follows: 4g zinc acetate, 3g vitamin C are dissolved in 100ml deionized water and stirred evenly under the action of a magnetic rotor, then ...

Embodiment 3

[0061] Step 1: PDMS modified clean cotton cloth.

[0062] In one embodiment, this step can be specifically performed as follows: First cut several pieces of the fabric according to the size of 3×3cm, put them in a beaker, pass through deionized water once, and ultrasonicate with absolute ethanol for 5 minutes, and put it in an oven at 80°C after ultrasonication Dry and cool for later use. Dissolve 7ml of PDMS in 500ml of tetrahydrofuran, continue to stir for 1 hour under the action of a magnetic rotor, add to the solution, wash with water and absolute ethanol in sequence, and dry the spare fabric, soak for 2 minutes; take it out and dry it at 100°C.

[0063] Step 2: the oil bath method is used to prepare the fabric with the surface of the nanometer ZnO particle layer.

[0064] In one embodiment, this step can be specifically performed as follows: 5g zinc acetate, 4g vitamin C are dissolved in 100ml deionized water and stirred evenly under the action of a magnetic rotor, then ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention discloses a production method of ZnO nanometer material fabric and the ZnO nanometer material fabric. The production method comprises following steps: (1), fabric is soaked in a PDMS (polydimethylsiloxane) solution and then is taken out and dried; (2), zinc acetate and vitamin C are dissolved in water and stirred uniformly, a first solution is prepared, an aqueous solution of sodium hydroxide is added to the first solution, a second solution is prepared, the fabric obtained in the step (1) is put in the second solution for a reaction, then the fabric is taken out, cleaned and dried, and the fabric with a ZnO nanoparticle layer is formed; (3), the fabric with the ZnO nanoparticle layer is soaked in the PDMS solution again, and then is taken out and dried. According to the production method of the ZnO nanometer material fabric and the ZnO nanometer material fabric, the operation is convenient and simple, the prepared ZnO nanoparticle layer is good in durability, and the problems of complicated preparation process, high time consumption, poor stability and mechanical property and the like of multiple traditional methods are solved.

Description

technical field [0001] The invention relates to the field of nanometer materials, in particular to a production method of a ZnO nanometer material fabric and a ZnO nanometer material fabric. Background technique [0002] Ultraviolet rays (UV for short) can be divided into long-wave ultraviolet UVA (320-400nm), medium-wave ultraviolet UVB (280-320nm) and short-wave ultraviolet UVC (200-280nm) according to the radiation wavelength. It is 290~400nm. The higher the UV light absorption and reflectivity on the fabric, the lower the UV transmittance and the better the protective performance of the product. At present, the mechanism of UV protection of textiles mainly comes from the absorption and shielding effect of the fiber fabric itself on ultraviolet rays, or the use of shielding agents to absorb and reflect ultraviolet rays. Excellent anti-ultraviolet performance can be obtained by the treatment of shielding agent. There are two main treatment methods: one is to add inorgani...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06M15/643D06M11/44
CPCD06M11/44D06M15/643
Inventor 赖跃坤朱天雪黄剑莹
Owner NANTONG TEXTILE & SILK IND TECH RES INST