Caprolactam pipeline cleaning system and method

A technology of caprolactam and cleaning system, applied in the field of cleaning system of caprolactam pipeline, can solve the problems of damage to pipeline and polymerization reaction tower, difficult pressure control, pollution of pipeline raw materials, etc., so as to reduce product rejection rate, avoid potential safety hazards, The effect of solving security risks

Active Publication Date: 2019-04-23
CHANGLE LIHENG POLYAMIDE TECH +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The nylon heater is a device that gradually heats caprolactam at a lower temperature to 235°C. Because of changing the formula, opening a new project, and short-term repairs due to equipment problems, the polymerization reaction tower needs to be carried out. Every time it stops, the pre-heater will There is caprolactam residue, and the residual caprolactam will undergo polymerization reaction, causing pipe blockage, resulting in damage to the heater, causing losses, or affecting the service life of the heater, whether the second start-up is smooth, and the quality of the final product
[0003] The current cleaning method is usually to manually connect a 2.5bar steam pipe before the pre-heater, and blow the caprolactam in the pre-heater into the pre-polymerization reaction tower when the car is parked. Manually taking over the pipe has potential safety hazard

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  • Caprolactam pipeline cleaning system and method

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Embodiment Construction

[0027] see figure 1 As shown, the present invention provides a technical solution: a cleaning system for a caprolactam pipeline. The caprolactam pipeline includes a caprolactam feeding pipeline 1, a production pipeline 7, a heater 71 and a polymerization tower 8. The cleaning system includes a cleaning pipeline 3. The outlet of the cleaning pipeline 3 is connected to the production pipeline 7, and the inlet of the cleaning pipeline 3 is respectively connected with the steam inlet pipe 2 which can be opened and closed and the inert gas inlet pipe 4 which can be controlled to be opened and closed. The cleaning pipeline 3 An overpressure protection valve 31 is set on the above, and a pressure sensor 5 is also set in the polymerization reaction tower 8, and the pressure sensor 5 and the overpressure protection valve 31 are respectively electrically connected to the controller 9 to automatically control the pressure threshold and protect the polymerization The safety of the reactio...

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Abstract

The invention discloses a caprolactam pipeline cleaning system and method in the technical field of caprolactam cleaning. The cleaning system comprises a caprolactam pipeline and a cleaning pipe, wherein the caprolactam pipeline comprises a caprolactam feeding pipe, a production pipeline, a heater and a polymerization tower; an outlet of the cleaning pipe is connected with the production pipeline;and an inlet of the cleaning pipe communicates with a steam inlet pipe capable of controlling opening and closing and an inert gas inlet pipe capable of controlling opening and closing. In actual production, problems are discovered, and a new system is made to protect existing equipment; through a controller, a pressure sensor and an overvoltage protecting valve, the pressure in the polymerization tower is preferably controlled; all systems are closed pipe systems, so that the manual flushing of pipelines and equipment is not needed, and the potential safety hazards of scald can be preferablyprevented; the equipment is protected; the risk is reduced; and the potential safety hazards caused by higher voltage are preferably solved.

Description

technical field [0001] The invention relates to the technical field of caprolactam cleaning, in particular to a cleaning system and method for a caprolactam pipeline. Background technique [0002] The nylon heater is a device that gradually heats caprolactam at a lower temperature to 235°C. Because of changing the formula, opening a new project, and short-term repairs due to equipment problems, the polymerization reaction tower needs to be carried out. Every time it stops, the pre-heater will There is caprolactam residue, and the residual caprolactam will undergo polymerization reaction, causing pipeline blockage, resulting in damage to the heater, causing losses, or affecting the service life of the heater, whether the second start-up is smooth, and the quality of the final product. [0003] The current cleaning method is usually to manually connect a 2.5bar steam pipe before the pre-heater, and blow the caprolactam in the pre-heater into the pre-polymerization reaction tow...

Claims

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Application Information

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IPC IPC(8): B08B9/032B08B13/00
CPCB08B9/0321B08B9/0325B08B13/00
Inventor 王兴镇
Owner CHANGLE LIHENG POLYAMIDE TECH
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