A long-lasting antibacterial material, a dental film and a long-lasting clear aligner
An antibacterial material and long-acting technology, applied in the field of dental diaphragms, long-acting invisible appliances, and long-acting antibacterial materials, can solve the problems of increased plaque adhesion, general antibacterial effect, imbalance of microorganisms in the plaque, etc. Physical fitness, strong antibacterial effect
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Embodiment 1
[0045] A kind of long-acting antibacterial material, comprises PETG resin and modified tourmaline; Wherein, the mass ratio of PETG resin and modified tourmaline is 30:1;
[0046] The preparation method of described modified tourmaline is:
[0047] Step S1. After the nano-tourmaline is treated with concentrated sulfuric acid, porous nano-tourmaline is obtained;
[0048] Step S2. After the porous nano-tourmaline is treated with glycerin, hydroxylated porous nano-tourmaline is obtained;
[0049] Step S3. Grafting hydroxylated porous nano tourmaline with limonoid to obtain modified tourmaline.
[0050] The nano tourmaline is colorless nano tourmaline.
[0051] The particle size of the nano tourmaline is 20-300nm.
[0052] In the step S1, the preparation method of the porous nano tourmaline is:
[0053] A1. Weigh the nano-tourmaline and add it to the reaction vessel, add concentrated sulfuric acid with a mass fraction of 70-80% dropwise into the reaction vessel, after the addit...
Embodiment 2
[0075] A long-acting antibacterial material, comprising PETG resin and modified tourmaline; wherein, the mass ratio of PETG resin and modified tourmaline is 10:1;
[0076] The preparation method of described modified tourmaline is:
[0077] Step S1. After the nano-tourmaline is treated with concentrated sulfuric acid, porous nano-tourmaline is obtained;
[0078] Step S2. After the porous nano-tourmaline is treated with glycerin, hydroxylated porous nano-tourmaline is obtained;
[0079] Step S3. Grafting hydroxylated porous nano tourmaline with limonoid to obtain modified tourmaline.
[0080] The nano tourmaline is colorless nano tourmaline.
[0081] The particle size of the nano tourmaline is 20-300nm.
[0082] In the step S1, the preparation method of the porous nano tourmaline is:
[0083] A1. Weigh the nano-tourmaline and add it to the reaction vessel, add concentrated sulfuric acid with a mass fraction of 70-80% dropwise into the reaction vessel, after the addition is ...
Embodiment 3
[0105] A long-acting antibacterial material, including PETG resin and modified tourmaline; wherein, the mass ratio of PETG resin and modified tourmaline is 10-50:1;
[0106] The preparation method of described modified tourmaline is:
[0107] Step S1. After the nano-tourmaline is treated with concentrated sulfuric acid, porous nano-tourmaline is obtained;
[0108] Step S2. After the porous nano-tourmaline is treated with glycerin, hydroxylated porous nano-tourmaline is obtained;
[0109] Step S3. Grafting hydroxylated porous nano tourmaline with limonoid to obtain modified tourmaline.
[0110] The nano tourmaline is colorless nano tourmaline.
[0111] The particle size of the nano tourmaline is 20-300nm.
[0112] In the step S1, the preparation method of the porous nano tourmaline is:
[0113] A1. Weigh the nano-tourmaline and add it to the reaction vessel, add concentrated sulfuric acid with a mass fraction of 70-80% dropwise into the reaction vessel, after the addition i...
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