Hologram recording material and hologram recording medium
一种全息照相、记录材料的技术,应用在全息图记录材料、记录载体材料、记录信息存储等方向,能够解决记录不均匀、基体单一等问题,达到容易设计、柔软性优越、相溶性良好的效果
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Embodiment 1
[0080] Using diphenyldimethoxysilane and a titanium butoxide polymer represented by the following structural formula, a holographic recording material was produced by the sol-gel method in the following steps.
[0081]
[0082] (Synthesis of organometallic compounds)
[0083] 7.8 g of diphenyldimethoxysilane and 7.2 g of a titanium butoxide polymer (manufactured by Nippon Soda, B-10) were mixed in 40 mL of a tetrahydrofuran solvent to prepare an alkoxide solution. That is, the molar ratio of Si and Ti is 1:1.
[0084] A solution consisting of 2.1 mL of water, 0.3 mL of 1N aqueous hydrochloric acid solution, and 5 mL of tetrahydrofuran was dropped into the alkoxide solution at room temperature while stirring, and the stirring was continued for 2 hours to carry out a hydrolysis reaction. Thus, a sol solution of an organometallic compound containing Si:Ti:phenyl=1:1:2 (molar ratio) was obtained.
[0085] (photopolymerizable compound)
[0086] 3 parts by weight of IRG-784 (C...
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