Petroleum ether extracted red tea extract, preparation and application thereof

A technique of petroleum ether extraction and petroleum ether, which is applied in the field of tobacco additive preparation, to achieve the effects of simple extraction process, coordination of cigarette aroma, and simple process

Active Publication Date: 2011-02-02
HONGYUN HONGHE TOBACCO (GRP) CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

If the excellent properties of black tea can be combined with cigarettes, it should be able to solve the above problems well, but there is no relevant report in the prior art

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] Weigh 500 grams of black tea with an electronic balance, put it into a flask, add 2500ml of medical grade petroleum ether with a boiling point of 30-60°C, soak for 10 hours at 20°C, separate the solid and liquid with a Bush funnel, collect the clear liquid, and obtain The liquid was distilled and concentrated for 2.0 h at a vacuum of 0.05 MPa and a distillation temperature of 28° C., and the solvent was removed to obtain 0.32 g of extract.

Embodiment 2

[0030] Weigh 1000 grams of black tea with an electronic balance, put it into an Erlenmeyer flask, add 10000ml of petroleum ether with a boiling point of 60-90°C, soak for 20 hours at 30°C, separate the solid and liquid with a Bush funnel, collect the clear liquid, and obtain the liquid in Distill and concentrate for 1.0 h at a vacuum of 0.1 MPa and a distillation temperature of 30° C., and remove the solvent to obtain 2.25 g of extract.

Embodiment 3

[0032] Weigh 1000 grams of black tea with an electronic balance, put it into an Erlenmeyer flask, add 15000ml of petroleum ether with a boiling point of 30-60°C, soak at 15°C for 10 hours, separate the solid and liquid with a Bush funnel, collect the clear liquid, and dilute the obtained liquid , Distill and concentrate for 1.5h under the conditions of vacuum degree of 0.01MPa and distillation temperature of 25°C, and remove the solvent to obtain 2.20 g of extract.

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Abstract

The invention discloses a red-tea alcohol extract extracted from petroleum ether as well as a preparation method and applications thereof. The red-tea is uniformly mixed with the petroleum ether and then a product is manufactured after the processes of extraction, solid-liquid separation, distilling and condensing are carried out on the mixture of the red-tea and the petroleum ether. The alcohol of 95 percent used for the red-tea alcohol extract extracted from petroleum ether is diluted to a concentration of 1 to 10 percent; then is added into the cigarette filaments according to 0.01 to 0.1 percent of the weight of the cigarette filaments for endowing special fragrance for the tobacco Simultaneously, free amino acids in the red-tea can better participle in a maillard reaction during the alcoholizing and burning process of the tobacco to generate a flavor matter and can neutralize the alkaline matters in the tobacco, thereby reducing stimulation, enriching the fragrance of the cigarette, lessening the stimulation and unpurified gases as well as improving the taste and aftertaste. The technique of the invention is simple; the operation is simple and convenient; besides, the existing production technique is not needed to be changed; the product does not have a solvent pollution; therefore, the red-tea alcohol extract has an excellent application prospect.

Description

technical field [0001] The invention belongs to the technical field of tobacco additive preparation, and in particular relates to a black tea extract extracted from petroleum ether. At the same time, the invention also relates to the preparation method of the extract and its application in cigarettes. Background technique [0002] Black tea is fermented tea, known as "black tea" in history. The chemical composition of its fresh leaves changes greatly during the processing, tea polyphenols are reduced by more than 90%, and new components such as theaflavins and thearubigins are produced. Aroma substances have increased from more than 50 kinds in fresh leaves to more than 300 kinds, and a part of caffeine, catechin and theaflavins are complexed into delicious complexes, thus forming its red soup, red leaves, sweet and mellow flavor. quality characteristics. On May 13, 2002, the American Medical Association published the research results of 497 men and 540 women citing black...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A24B15/28A24B3/12C11B9/00
Inventor 李祖红朱保昆黄立斌李庆华夏建军者为
Owner HONGYUN HONGHE TOBACCO (GRP) CO LTD
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