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Composite active black dye

A technology of reactive black and dyes, applied in the field of dyes, can solve the problems of insufficient blackness, difficulty in ensuring level dyeing and reproducibility, etc., and achieve good color fixing ability, small difference between dyeing rate and color fixing rate, The effect of high depletion ratio

Active Publication Date: 2012-12-12
HUBEI HUALI DYESTUFF INDAL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] In recent years, the printing and dyeing industry has adopted the most widely reactive black, and most of them are compounded by adding C.I reactive orange 78 to C.I reactive black 5. Although the principle of complementary color has been used to improve the blackness of commercial dyes, it is still in the dyeing process. There are still several shortcomings: ①The blackness is not full enough; ②Because C.I reactive black 5 and C.I reactive orange 78 contain different types of active groups, the directness of the two to the fiber, dyeing temperature, bath ratio, and dyeing accelerator There are large individual differences in the sensitivity of salts, color fixing agent alkalis, and pH value, so it is difficult to guarantee level dyeing and reproducibility; ③A certain application performance needs to be improved, such as color fixing rate, solubility, lifting rate, Dyeing depth, rubbing fastness, etc.

Method used

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  • Composite active black dye
  • Composite active black dye
  • Composite active black dye

Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0022] 82 parts of formula (1) dyes, 8 parts of formula (2) dyes, 2 parts of formula (3) dyes, 8 parts of formula (4) dyes are fully mechanically mixed to obtain the composite reactive black dye of the present invention.

[0023] Dyeing Instructions

[0024] Dyeing Instructions 1

[0025] Dissolve 1 g of the dye prepared in the above-mentioned manner with an appropriate amount of water, and then set the volume in a 250ml volumetric flask. Draw 50ml of dye solution and mix it with 50ml of water, then add 5g of cotton cloth and 6g of sodium sulfate, then raise the temperature to 60°C at a rate of 1°C / min, keep it for 30 minutes, add 2g of sodium carbonate, and keep it at 60°C for 30 minutes, then Take out the cotton cloth to be dyed, boil it with non-ionic detergent boiling soap for 15 minutes, then wash it with water and dry it at about 70 ℃, the result is better than KN-GRC black, BED black and ARC black, with better level dyeing property and washing fastness , jet blackness...

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PUM

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Abstract

The invention relates to a composite active black dye, which is characterized in that the dye is compounded by four dyes shown in formula (1), formula (2), formula (3) and formula (4) according to parts by weight of 80-84, 6-10, 1-3 and 6-10, has high responsiveness, good color fixing capability and excellent deep dyeing property, and is suitable for dyeing cotton fiber.

Description

technical field [0001] The invention relates to a dye, especially a composite reactive black dye. Background technique [0002] In recent years, the printing and dyeing industry has adopted the most widely reactive black, and most of them are compounded by adding C.I reactive orange 78 to C.I reactive black 5. Although the principle of complementary color has been used to improve the blackness of commercial dyes, it is still in the dyeing process. There are still several shortcomings: ①The blackness is not full enough; ②Because C.I reactive black 5 and C.I reactive orange 78 contain different types of active groups, the directness of the two to the fiber, dyeing temperature, bath ratio, and dyeing accelerator There are large individual differences in the sensitivity of salts, color fixing agent alkalis, and pH value, so it is difficult to guarantee level dyeing and reproducibility; ③A certain application performance needs to be improved, such as color fixing rate, solubility...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09B67/24C09B67/36D06P1/38D06P3/66
Inventor 艾良军尚爱国崔孟元李华龙殷德华
Owner HUBEI HUALI DYESTUFF INDAL
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