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Identification method of herba patriniae in Chinese herbal compound

A technology of sagebrush and traditional Chinese medicine, which is applied in the preparation, sampling, measuring device and other directions of test samples, can solve the problems of poor separation effect and undetectable, and achieve the effect of good separation effect, excellent effect and simple method.

Active Publication Date: 2017-03-15
HEBEI KEHENG BIOTECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The applicant once used the identification methods in the literature to carry out thin-layer chromatography identification of Patrinia in Baikubai Li Oral Liquid, and the results showed that these methods could not be detected, and the separation effect was not good

Method used

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  • Identification method of herba patriniae in Chinese herbal compound
  • Identification method of herba patriniae in Chinese herbal compound
  • Identification method of herba patriniae in Chinese herbal compound

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0049] The identification method of Patrinia in the Chinese medicine compound of the present embodiment is the thin-layer chromatography identification of Patrinia in Longqing Tablets:

[0050] 1. Instruments and reagents

[0051] Patrinia control medicinal materials (National Institute for the Control of Pharmaceutical and Biological Products, batch number: 121271-201201); medicinal materials used in the prescription (purchased from Hebei Anguo Traditional Chinese Medicinal Materials Market); Longqing Tablets (Tianjin Zhongxin Pharmaceutical Group Co., Ltd. Longshunrong Pharmaceutical Factory, specifications: each piece weighs 0.6 g, batch number: 20130226); silica gel G plate (100mm×100mm, Qingdao Ocean Chemical Factory); other reagents are analytically pure.

[0052] 2. Methods and Results

[0053] (1) Preparation of contrast medicinal material solution: get Patrinia reference medicinal material 2g, add water 150ml, decoct for half an hour, filter, filtrate is concentrated...

Embodiment 2

[0061] The identification method of Patrinia in the Chinese medicine compound of the present embodiment is the thin-layer chromatography identification of Patrinia in Qianlieping Capsules:

[0062] 1. Instruments and reagents

[0063] Patrinia control medicinal materials (National Institute for the Control of Pharmaceutical and Biological Products, batch number: 121271-201201); medicinal materials used in prescriptions (purchased in Hebei Anguo Traditional Chinese Medicinal Materials Market); Qianlieping Capsules (Xi’an Qianhe Pharmaceutical Co., Ltd., specification: 0.4g / grain, batch number: 20140702); silica gel G plate (100mm×100mm, Qingdao Ocean Chemical Factory); other reagents were of analytical grade.

[0064] 2. Methods and Results

[0065] (1) Preparation of contrast medicinal material solution: get Patrinia reference medicinal material 2g, add water 150ml, decoct for half an hour, filter, filtrate is concentrated to 30ml, prepare with need testing solution prepara...

Embodiment 3

[0073] The identification method of Patrinia in the Chinese medicine compound of the present embodiment is the thin-layer chromatography identification of Patrinia in Jinmagantai granules:

[0074] 1. Instruments and reagents

[0075] Patrinia reference medicinal material (National Institute for the Control of Pharmaceutical and Biological Products, batch number: 121271-201201); medicinal materials used in the prescription (purchased at Hebei Anguo Traditional Chinese Medicine Market); Jinma Gantai Granules (Guizhou Changshou Changle Pharmaceutical Factory, specifications: 2g per bag (no sucrose), batch number: 20160301); silica gel G plate (100mm×100mm, Qingdao Ocean Chemical Factory); other reagents were of analytical grade.

[0076] 2. Methods and Results

[0077] (1) Preparation of contrast medicinal material solution: get Patrinia reference medicinal material 2g, add water 150ml, decoct for half an hour, filter, filtrate is concentrated to 30ml, prepare with need testing...

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Abstract

The invention discloses an identification method of herba patriniae in a Chinese herbal compound, and particularly relates to a thin-layer identification method of herba patriniae in a Chinese herbal compound. The identification method comprises the following steps of preparing a reference crude drug solution; preparing a test product solution; preparing a negative sample solution; performing sample application on the same silica gel G thin-layer plate with a capillary sample applicator; placing the thin-layer plate into a chromatographic jar, performing expansion with an expanding agent, taking out and drying the thin-layer plate in air; and inspecting a thin-layer chromatographic sheet to obtain a result for identification, wherein a main spot of the same color is developed at a position, which corresponds to a reference crude drug chromatography, on a test product chromatography, but no spot is developed on a negative sample. The identification method disclosed by the invention is simple in technology, good in separation effect and extremely high in specificity; and the accuracy of component identification of herba patriniae in the Chinese herbal compound is further improved, and the identification method has a huge popularization and application potential in the field of identification of herba patriniae-related medicines.

Description

technical field [0001] The invention relates to a method for identifying Patrinia in compound Chinese medicines, in particular to a TLC identification method for Patrinia in compound Chinese medicines. Background technique [0002] It is the dried whole plant of Patrinia scabiosaefolia Fisch. or Patrinia villosa Juss. of Patrinaceae. In summer, the flowers are collected before they bloom, dried in the sun until they are half-dried, tied into bundles, and then dried in the shade. Mainly produced in Jiangsu, Zhejiang, Hubei, Anhui. Patrinia has the effects of clearing heat and detoxifying, removing blood stasis and draining pus. Indications for appendicitis, dysentery, enteritis, hepatitis, conjunctivitis, postpartum blood stasis and abdominal pain, carbuncle and furuncle. Patrinia can also be combined with other medicinal materials to make a variety of compound Chinese medicines, such as Longqing Tablets recorded in a 2015 article, Patrinia Tablets, Fufang Fuyanping Capsul...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/90G01N1/40
CPCG01N1/4022G01N1/4055G01N30/90G01N2001/4061
Inventor 牛卫宁梁冰尹朋张磊
Owner HEBEI KEHENG BIOTECH
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