A kind of preparation method of low-carbon mixed gas hydrate explosion suppressing agent
A technology of mixed gas and hydrate, applied in chemical instruments and methods, other chemical processes, etc., can solve the problems of pure carbon dioxide explosion suppressant with strong greenhouse effect, no public report on explosion-proof materials, and poor explosion suppression effect, etc. Achieving the effects of abundant raw materials, good explosion suppression effect and low cost
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Embodiment 1
[0019] In the specific implementation of the present invention, a preparation method of a low-carbon mixed gas hydrate explosion suppressing agent comprises the following steps:
[0020] (1) Preparation of hydration agent:
[0021] adding the inorganic salt silicon dioxide into the water so that the mass content of the silicon dioxide is 0.05mol / L;
[0022] (2) Preparation of inert mixed gas:
[0023] The inert mixed gas is composed of a mixture of 10% carbon dioxide, 90% nitrogen and argon, and the volume ratio of nitrogen and argon is 1:1;
[0024] (3), mixed reaction:
[0025] Fill the inert mixed gas into the hydration agent, make the pressure reach 7MPa, and react at 3°C for 150 minutes to form mixed gas hydrate, and crush the mixed gas hydrate formed by the reaction below -10°C into particles with a particle size of less than 1.0mm Hydrate powder and serve.
Embodiment 2
[0027] In the specific implementation of the present invention, a preparation method of a low-carbon mixed gas hydrate explosion suppressing agent comprises the following steps:
[0028] (1) Preparation of hydration agent:
[0029] Add the inorganic salt NaCl to the dry water so that the mass content of NaCl is 0.01mol / L;
[0030] (2) Preparation of inert mixed gas:
[0031] The inert mixed gas is composed of a mixture of 7% carbon dioxide, 93% nitrogen and argon by volume, and the volume ratio of nitrogen to argon is 1:3;
[0032] (3), mixed reaction:
[0033] Fill the inert mixed gas into the hydration agent, make the pressure reach 6MPa, and react at 1°C for 160 minutes to generate mixed gas hydrate, and crush the mixed gas hydrate formed by the reaction into particles with a particle size of less than 1.0mm at a temperature below -10°C Hydrate powder and serve.
Embodiment 3
[0035] In the specific implementation of the present invention, a preparation method of a low-carbon mixed gas hydrate explosion suppressing agent comprises the following steps:
[0036] (1) Preparation of hydration agent:
[0037] adding the inorganic salt MgF into the dry solvent water, so that the mass content of the inorganic salt is 0.03mol / L;
[0038] (2) Preparation of inert mixed gas:
[0039] The inert mixed gas is composed of a volume ratio: 14% of carbon dioxide, 86% of a mixture of nitrogen and argon, and the nitrogen and argon are in any volume ratio;
[0040] (3), mixed reaction:
[0041] Fill the inert mixed gas into the hydration agent, make the pressure reach 8MPa, react at -10-5°C for 100-240min to form mixed gas hydrate, and crush the mixed gas hydrate formed by the reaction below -10°C into granules Hydrate powder with a diameter less than 1.0mm is ready.
[0042] As can be seen from the above, the present invention is a preparation method of a low-carb...
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