A kind of choline chloride feed additive and preparation method thereof
A feed additive, choline chloride technology, applied in the field of feed additives, can solve the problems of oxidation of choline chloride feed additives, and achieve the effects of improving immunity and anti-stress ability, preventing animal constipation, and preventing oxidation.
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Embodiment 1
[0026] A choline chloride feed additive comprises the following components in parts by weight: 50 parts of choline chloride, 1 part of chitosan chloride and 10 parts of bean dregs powder.
[0027] A kind of preparation method of choline chloride feed additive is characterized in that: comprises the following steps:
[0028] (1) Take by weighing 50 parts of choline chloride, 1 part of chitosan chloride, and 10 parts of bean dregs powder;
[0029] (2) Dissolve 1 part of chlorinated chitosan in 60mL of 5% acetic acid solution, stir well to obtain chitosan acetic acid solution, and let it stand for 30mM;
[0030] (3) Add 50 parts of choline chloride to the chitosan acetic acid solution to obtain a mixed solution;
[0031] (4) Add 10 parts of bean dregs powder to the mixed solution, then heat it in a constant temperature water bath at 60°C for 7 hours, filter it under reduced pressure, wash it with absolute ethanol and distilled water for 3 times, and dry it in vacuum at 60°C for ...
Embodiment 2
[0033] A choline chloride feed additive comprises the following components in parts by weight: 60 parts of choline chloride, 2 parts of chitosan chloride and 13 parts of bean dregs powder.
[0034] A kind of preparation method of choline chloride feed additive is characterized in that: comprises the following steps:
[0035] (1) Take by weighing 60 parts of choline chloride, 2 parts of chitosan chloride, and 13 parts of bean dregs powder;
[0036] (2) Dissolve 2 parts of chlorinated chitosan in 80mL5% acetic acid solution, stir to obtain chitosan acetic acid solution, leave standstill for 30mM;
[0037] (3) Add 60 parts of choline chloride to the chitosan acetic acid solution to obtain a mixed solution;
[0038] (4) Add 13 parts of bean dregs powder to the mixture, then heat it in a constant temperature water bath at 70°C for 7.5 hours, filter it under reduced pressure, wash it with absolute ethanol and distilled water for 3 times, and dry it in vacuum at 65°C for 4 hours to ...
Embodiment 3
[0040] A choline chloride feed additive comprises the following components in parts by weight: 70 parts of choline chloride, 3 parts of chitosan chloride and 15 parts of bean dregs powder.
[0041] A kind of preparation method of choline chloride feed additive is characterized in that: comprises the following steps:
[0042] (1) Take by weighing 70 parts of choline chloride, 3 parts of chitosan chloride, and 15 parts of bean dregs powder;
[0043] (2) Dissolve 3 parts of chlorinated chitosan in 100mL5% acetic acid solution, stir to obtain chitosan acetic acid solution, leave standstill for 30mM;
[0044] (3) Add 70 parts of choline chloride to the chitosan acetic acid solution to obtain a mixed solution;
[0045] (4) Add 15 parts of bean dregs powder to the mixed solution, then heat in a constant temperature water bath at 80°C for 8 hours, filter under reduced pressure, wash with absolute ethanol and distilled water for 3 times, and dry in vacuum at 70°C for 5 hours to finall...
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