A method for preparing zeolite molecular sieves by rapid crystallization of dry glue
A zeolite molecular sieve and molecular sieve technology, which are applied in chemical instruments and methods, crystalline aluminosilicate zeolite, octahedral crystalline aluminosilicate zeolite, etc., can solve problems such as low crystallinity and impure crystal phase, and achieve crystallization time Short, short crystallization cycle, the effect of shortening the production cycle
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Embodiment 1
[0036] Get 1 ton of NaY crystallization mother liquor produced when catalyst factory is produced, wherein NaY 2 O mass fraction is 4.2%, SiO 2 The mass fraction is 20%; according to the proportion of the directing agent is 1Al 2 o 3 : 8SiO 2 : 0.01F - Add the following raw materials: pseudo-boehmite (65.5wt%, Aluminum Corporation of China Shanxi Aluminum Plant) 64.88kg, NH 4 F (96wt%, Tianjin Kemiou Reagent Co., Ltd.) 0.16kg was crystallized in a crystallization kettle at 90°C for 2 hours to obtain a directing agent for use.
[0037] Add the following raw materials to the guide agent: sodium hydroxide (chemically pure, content ≥96.0%, Tianjin Kemiou Chemical Reagent Development Center) 36.98kg, white carbon black (industrial grade, content ≥97.0%, Shanxi Tongde Chemical Co., Ltd. company) 51.54kg. Finally, dry glue powder was made after flash drying at 90°C.
[0038] With the prepared dry rubber powder, in the solid phase continuous reactor (such as figure 1 ) Add 1000...
Embodiment 2
[0046] Get 1 ton of NaY crystallization mother liquor produced when catalyst factory is produced, wherein NaY 2 O mass fraction is 4.2%, SiO 2 The mass fraction is 30%; according to the ratio of the directing agent is 1Al 2 o 3 : 5SiO 2 : 0.1F - Add the following raw materials: pseudoboehmite (Al 2 o 3 The content is 65.5wt%, Aluminum Corporation of China Shanxi Aluminum Plant) 155kg, NH 4 3.85kg of F (96wt%, Tianjin Kemiou Reagent Co., Ltd.) was crystallized in a crystallization kettle at 90°C for 10 hours to obtain a directing agent for use.
[0047] Adding raw materials to the guide agent: sodium hydroxide (chemically pure, content ≥96.0%, Tianjin Kemiou Chemical Reagent Development Center) 602kg, white carbon black (industrial grade, content ≥97.0%, Shanxi Tongde Chemical Co., Ltd.) 927kg. The prepared gel was finally dried at 90°C to make dry gel powder.
[0048] With the prepared dry rubber powder, in the solid phase continuous reactor (such as figure 1 ) Add 5...
Embodiment 3
[0054] Another batch of NaY type molecular sieve crystallization mother liquor 1 ton produced when getting catalyst factory production, wherein NaY 2 The mass fraction of O is 5.4%: SiO 2 The mass fraction is 25%; according to the ratio of the directing agent is 1Al 2 o 3 : 4SiO 2 : 0.05F - Add the following raw materials: pseudoboehmite (Al 2 o 3 The content of NaF is 65.5wt%, Aluminum Corporation of China (Shanxi Aluminum Factory) 162kg, NaF (98wt%, Tianjin Jinke Fine Chemical Research Institute) 2.28kg, crystallized in the crystallization kettle at 90°C for 5h to obtain the directing agent.
[0055] Add raw materials to the guiding agent: sodium hydroxide (chemically pure, content ≥ 96.0%, Tianjin Kemiou Chemical Reagent Development Center) 213kg, silica sol (25wt%, Qingdao Ocean Chemical Co., Ltd.) 2750kg. Finally, it is dried at 90°C to make dry rubber powder.
[0056] The dry rubber powder was crystallized at 100°C for 10 hours in a water vapor atmosphere in a spe...
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