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Catalyst distillation component and catalyst distillation method used said component

A catalytic distillation and component technology, applied in chemical instruments and methods, fractionation, chemical/physical processes, etc., can solve the problems of high catalyst strength requirements, affecting mass transfer and reaction effects, and high production technical requirements, to overcome mass transfer. Reduced effect, good liquid redistribution ability, high catalytic reaction efficiency

Inactive Publication Date: 2006-09-13
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The disadvantage of this component is: the catalyst is solid, so the particle size cannot be too large, otherwise the catalyst cannot be fully utilized, but the catalyst particle size is too small and it is easy to be stratified with the filler, which damages the component to perform its catalytic reaction-distillation separation Synergy function , In addition, this component is also prone to channeling in the bed, which affects its mass transfer and reaction effects
This kind of component has high mass transfer efficiency, good catalyst utilization rate and good product selectivity, but it has high requirements on the strength of the catalyst and high requirements on the production technology of the catalyst and packing. During the operation, the catalyst and packing are easy to separate, thus Causes large local resistance and affects the flux of gas and liquid

Method used

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  • Catalyst distillation component and catalyst distillation method used said component
  • Catalyst distillation component and catalyst distillation method used said component
  • Catalyst distillation component and catalyst distillation method used said component

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Embodiment

[0051] The catalytic distillation assembly of the present invention is used for C 3 Catalytic distillation to remove MPEA MAPD The industrial side line experimental device, the material composition is shown in Table 1, the temperature: 105-40 °C, the pressure 1.9Mpa, the diameter of the industrial side line device is 300mm, and the height is 23000mm. The catalytic distillation assembly of the present invention is made into an integral assembly with a diameter of 300mm and a height of 220mm. The catalyst used in the catalytic distillation assembly adopts the solid ball BC series hydrogenation catalyst with a diameter of φ3mm produced by the Beijing Research Institute of Chemical Industry. The wire mesh container of the catalyst is 13mm in diameter plane wire mesh cylinder, the length is the same as the length of the free channel of the filler of the present invention, the filler plate is made of stainless steel corrugated plate with a pattern pressed on the surface, the wave d...

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Abstract

The invention discloses a kind of catalyst distillation module and uses this module the catalyst distillation method.The invention catalyst distillation module includes the granules of catalyst, the silk screen vessel and the filler plate, its characteristic lies in, in the stated silk screen vessel which is used to load and fill granules of catalyst one by one or interval lays to the stated free channel which is formed by fold put the filler plate;Among them the stated filler plate is the corrugated sheet padding,open arbitrary shape holes on the corrugated sheet trough,remove the open hole part on the stated corrugated sheet, or divides the hole opened part into two parts along the ripple direction, then move upward or downward the formed two teeth pieces.The invention module has the force fluid redistribute ability, overcame the flaw that channel and so on cause the mass transfer effect droppes ; Lengthenes the fluid mobile way, increases the hold liquid volume of the reaction zone liquid.

Description

technical field [0001] The present invention relates to a kind of equipment and method of chemical engineering and catalytic reaction engineering, especially to a new component of catalytic distillation tower and its application in gas-liquid, liquid-solid, liquid-liquid-solid, gas-liquid-solid Methods in Catalytic Distillation Reactions. Background technique [0002] In the fields of chemical industry, petrochemical industry, fine chemical industry, metallurgy and environmental engineering, there are many gas-liquid, liquid-solid, liquid-liquid-solid, gas - Liquid-solid system. These catalytic reaction systems are particularly suitable for carrying out by means of catalytic distillation. [0003] Catalytic distillation technology is a chemical engineering and catalytic reaction engineering technology developed in recent years. It combines catalytic reaction process and distillation refining technology, and simultaneously completes catalytic reaction process and distillati...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D3/32B01J8/04
Inventor 戴伟李振虎杨元一郭彦来王国清李东风廖丽华彭晖程建民
Owner CHINA PETROLEUM & CHEM CORP
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