The invention discloses a method for measuring
solid content of volatilization-inhibiting and protection organic
silicon slag slurry, which comprises the following steps: weighing a certain amount of organic
silicon slurry, adding an extracting agent, mixing, carrying out
centrifugal separation, separating
solid from liquid, recycling the used extracting agent at the upper layer through
distillation, adding a
separating agent into the
silicon slag at the lower layer, uniformly stirring, centrifuging again, and collecting the
solid content of the organic silicon
slag at the lower layer; and after solid-liquid separation, lower-layer silicon slag is dried in a
drying mode and then weighed, and finally the
solid content result of the silicon
slurry is obtained. By means of adding an extracting agent, a
separating agent and the like, the method aims at solving the problems of serious
distortion of measurement results, high operation risk, serious environmental
pollution and the like caused by violent volatilization and
hydrolysis of
chlorosilane monomers and uncontrollable
side reaction of the
chlorosilane monomers and reactive
hydrogen-containing solvents (such as alcohols) in the existing method for measuring the
solid content of the organic silicon slurry. Meanwhile, the extracting agent and the
separating agent can be recycled after high-boiling-point substances are separated in a
distillation mode, the method has the advantages of being easy to operate, good in
repeatability,
environmentally friendly and the like, multiple measurement results RSD are smaller than 1%, and the detection requirement is completely met.