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Sea water desalting agent based on silver carrying acid zeolite and its prepn process

A technology of acidic zeolite and silver-loaded zeolite, which is applied in seawater treatment, chemical instruments and methods, water/sewage treatment, etc. It can solve the problems of increasing the difficulty of effluent filtration, increasing the volume of chemicals, reducing the use efficiency, etc., and achieving the effect of seawater desalination Good, increase the silver loading, the effect of high silver loading

Inactive Publication Date: 2011-06-08
TIANJIN SEA WATER DESALINATION & COMPLEX UTILIZATION INST STATE OCEANOGRAPHI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For the problem that the pH value of the desalination agent obtained by this preparation method increases after seawater desalination, it was proposed in U.S. Patent No. 2,322,689 to neutralize excess hydroxide ions with citric acid to generate soluble sodium citrate, but pharmacological tests suggests that this has the potential to cause alkalosis and physiological dehydration
In U.S. Patent US 2,363,020, uric acid is used to reduce the pH value of the effluent to generate insoluble sodium urate, but it is found that this will increase the difficulty of filtering the effluent and affect the taste of the water
At present, people control the amount of silver oxide and barium hydroxide and add strong acid cation exchange resin to make the pH value of the effluent in the range of 8.9 to 10.5, but the volume of the agent is increased and the use efficiency is reduced.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0057] The desalination agent for seawater desalination based on acidic silver-loaded mordenite consists of 56 g of acidic silver-loaded mordenite, 2 g of silver oxide, 4 g of barium hydroxide, 0.5 g of montmorillonite, 0.6 g of stearic acid, and 0.2 g of activated carbon.

Embodiment 2

[0059] The desalination agent for seawater desalination based on acidic silver-loaded 4A zeolite is composed of: 52g of acidic silver-loaded 4A zeolite, 5g of silver oxide, 3g of barium hydroxide, 0.4g of montmorillonite, 0.6g of stearic acid, and 0.3g of activated carbon.

Embodiment 3

[0061] Embodiment 1 Preparation process of desalination agent for seawater desalination based on acidic silver-loaded mordenite:

[0062] Preparation of acidic zeolite: put 70g of mordenite in a closed container, evacuate to a vacuum of 2kPa, then add 1000ml of 0.1mol / L NH 4 NO 3 solution, stirred and exchanged at 80°C for 4h, filtered, washed with distilled water until no NO - 3 , Repeat this exchange three times, dry the powder at 120°C for 12 hours, and then roast at 300°C for 6 hours to obtain acidic mordenite.

[0063] Acidic zeolite impregnation with silver: put the acidic mordenite in a closed container, evacuate to a vacuum of 1kPa, then add 500ml of 0.3mol / L AgNO 3 Solution, after fully stirring and mixing evenly, stir and exchange at 80°C for 3h, filter and wash with distilled water until no Ag + , Repeat the exchange twice, and then dry at 60°C for 16 hours to obtain acidic silver-loaded mordenite.

[0064] Preparation of desalting agent by mixing: mix 56g of a...

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Abstract

The present invention relates to sea water desalting agent based on silver-carrying acid zeolite and its preparation process, and belongs to the field of sea water desalting technology. The sea water desalting agent based on silver-carrying acid zeolite consists of silver-carrying acid zeolite, silver oxide and barium hydroxide. Its preparation process includes the following steps: preparing acidzeolite through soaking zeolite in acid solution or ammonium salt solution for ion exchange at 25-80 deg.c, washing, filtering and stoving; preparing silver-carrying acid zeolite through soaking the acid zeolite in silver ion solution for ion exchange at 60-120 deg.c in heliophobic condition, washing, filtering and stoving; and mixing the silver-carrying acid zeolite, silver oxide and barium hydroxide in heliophobic condition to obtain the sea water desalting agent. The sea water desalting agent has high desalting efficiency, high effluent quality, simple preparation process and other advantages.

Description

technical field [0001] The invention belongs to the technical field of seawater desalination, and in particular relates to a seawater desalination agent based on silver-loaded acidic zeolite and a preparation method thereof. Background technique [0002] Sea water is bitter and cannot be drunk directly. Seawater salinity is mainly sodium chloride, accounting for about 78%, and the remaining 22% is magnesium chloride, magnesium sulfate, potassium chloride, etc. The salinity of human blood is 0.9%, while the salinity of seawater is as high as 4 times. If you drink seawater directly, the body will have too much salt, and the excess salt will be excreted by the kidneys in the form of urine, which may lead to dehydration and death. Therefore, seawater desalination agents must be carried in lifeboats or skydiving equipment to desalinate seawater to replenish water. [0003] At present, the existing seawater desalination agent is used as a chemical agent for desalinating seawate...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C02F1/00C02F1/28C02F103/08C02F1/58C02F1/66C02F1/42
Inventor 张雨山黄庆华曾兴宇王静杨雪姜天翔
Owner TIANJIN SEA WATER DESALINATION & COMPLEX UTILIZATION INST STATE OCEANOGRAPHI
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