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1994results about How to "Reduce precipitation" patented technology

Manufacturing process for the production of polypeptides expressed in insect cell-lines

The present invention provides a manufacturing method for polypeptides that are produced in insect cells using a baculoviral expression system. In one example, the insect cell culture is supplemented with a lipid mixture immediately prior to infection (e.g., one hour prior to infection). The polypeptides are isolated from the insect cell culture using a method that employs anion exchange or mixed-mode chromatography early in the purification process. This process step is useful to remove insect-cell derived endoglycanases and proteases and thus reduces the loss of desired polypeptide due to enzymatic degradation. In another example, mixed-mode chromatography is combined with dye-ligand affinity chromatography in a continuous-flow manner to allow for rapid processing of the insect-cell culture liquid and capture of the polypeptide. In yet another example, a polypeptide is isolated from an insect cell culture liquid using a process that combines hollow fiber filtration, mixed-mode chromatography and dye-ligand affinity in a single unit operation producing a polypeptide solution that is essentially free of endoglycanase and proteolytic activities. In a further example, the isolated polypeptides are glycopeptides having an insect specific glycosylation pattern, which are optionally conjugated to a modifying group, such as a polymer (e.g., PEG) using a glycosyltransferase and a modified nucleotide sugar.
Owner:NOVO NORDISK AS

Organic silicon rubber encapsulating material for high-power LED

The invention relates to an organic silicon encapsulating material for a high-power LED and a preparation method thereof. The organic silicon encapsulating material is prepared by mixing a component A containing vinyl polysiloxanes, a silicone resin component B, a component C containing hydrogen polysiloxane, a platinum catalyst component D, a component E of catalytic inhibitor of acetylene alcohols and a tackifier component F. The obtained encapsulating silicon rubber with different refractive indexes of level 1.4, level 1.5 and the like can be used for the encapsulation of various high-power LEDs and the encapsulation of other optical application. The organic silicon rubber encapsulating material for the high-power LED takes the silicone resin component B as a filling material, which not only enables that the silicone rubber has high transparency, high strength and high light transmittance, but also improves the temperature resistance, the yellowing resistance, and the durability of the high light transmittance of high-power LED products. The organic silicon rubber encapsulating material for the high-power LED can be prepared into two encapsulating forms of a single component and bi-component, which improves the adaptability and the encapsulating efficiency for encapsulating equipment and process procedures, and has the characteristics of reduced cost and convenient use.
Owner:陈俊光

Processing method of stainless steel cold rolling pickling wastewater

The invention relates to a processing method of stainless steel cold rolling pickling wastewater. The pickling wastewater enters a hexavalent chrome secondary reduction pool after the actions of micro-electrolysis and hexavalent chrome preliminary reduction of a scrap iron filtering pool; the reduced wastewater enters a front-segment precipitation tank after neutralization and aeration, heavy metal sludge is concentrated and dehydrated, and the heavy metal sludge and scrap iron after the use of the scrap iron filtering pool are recycled and used as stainless steel smelting raw materials; middle-segment precipitation is carried out after a primary supernatant acts with a precipitant, and dehydrated and dried fluoride sludge is recycled and used as a metallurgical adjuvant material; final-segment precipitation is carried out after a secondary supernatant continues to act with a flocculating agent to obtain calcium salt which can be used as a building material raw material; and after the three segments of precipitation of acidic wastewater, the final third level supernatant reaches a standard and is discharged through water quality regulation and sand filtering. The invention has the advantages of less investment, low wastewater processing cost, convenient maintenance and the like, and not only can effectively utilize discarded scrap iron of a stainless steel enterprise, but also can greatly lower the subsequent wastewater processing cost and the operating load.
Owner:BAOSHAN IRON & STEEL CO LTD

A method for the treatment and reuse of ammonia-nitrogen-containing high-salt catalyst wastewater

The invention relates to a recycling method for treating ammonia nitrogen containing high-salt catalyst wastewater by adopting a membrane separation technology. The process flow of 'acid regulation, micro-filtration, membrane distillation, cooling and crystallization' is adopted in the method. By adopting the process flow, salts, ammonia nitrogen and metal ions in the wastewater can be effectively removed, and deep treatment and recycle of the ammonia nitrogen containing high-salt catalyst wastewater are realized. The process flow makes full use of the technical advantages of membrane distillation, solves the problem that the discharge of high salts, ammonia nitrogen and metal ions of the ammonia nitrogen containing high-salt catalyst wastewater does not reach the standards, and realizes recycle of the produced water. After the ammonia nitrogen containing high-salt catalyst wastewater is treated by the process flow, the reclamation rate of the wastewater is more than 90 percent, and high recycle of the ammonia nitrogen containing high-salt catalyst wastewater is realized; and the method accords with the development strategies of energy conservation and emission reduction, and has remarkable social benefit and economic benefit.
Owner:CHINA PETROLEUM & CHEM CORP +1

Low-salt liquid state fermented soy sauce production process

The invention discloses a low-salt liquid state fermented soy sauce production process, comprising the following main processes: preparing koji in a koji-maker machine; mixing the wheat which is fried and smashed with koji, inoculating the mixture in soybean meal and bran which are cooked; preparing finished koji in a koji making disc machine; mixing the finished koji with brine, sending the mixture in a fermenting vat for fermentation; preparing the finished soy sauce through soaking, pouring oil, filtrating, mixing, sterilizing and filling to obtain the finished soy sauce. The soy sauce is characterized in that materials containing zygosaccharomyces Rouxii 2.180 accounting for 1.5-2.5% of the total weight of materials and torulopsis candida 2.202 accounting for 1.5-2.5% of the total weight of materials are added during the medium term of the fermentation process and the raw materials--soybean meal and bran are cooked by high temperature short-time continuous cooking process. Compared with the prior art, the raw material digestion rate can reach 88-90%, the protein utilization rate can reach 83%, the activity of neutral protease of the finished koji can reach 2000mu / g, the enzymesystem is complete, the defects such as long period of high-salt liquid state fermentation (180 days), burnt flavour and heavy bitter taste of low-salt solid state fermentation and the like are overcame and the produced soy sauce is characterized by strong soysauce-like aroma, alcohol-like aroma and ester-like aroma and the like.
Owner:QIANHE CONDIMENT & FOOD CO LTD

Preparation method of micro/nano-structure ultrahigh-strength plastic stainless steel containing Nb

The invention belongs to the field of production of ultrahigh-strength plastic alloy steel, and relates to a preparation method of micro/nano-structure ultrahigh-strength plastic stainless steel containing Nb. The preparation method comprises the steps of: firstly preparing materials according to a composition proportion, adding 0.05-0.15% of Nb element on the basis of 316L austenitic stainless steel, then carrying out vacuum induction furnace smelting, casting blank forging, forged piece hot rolling and solution treatment, carrying out cold deformation on the steel plate which undergoes the solution treatment with deformations of 40%, 60%, 80% and 90% and with single reduction in pass controlled within 3-10% to prepare steel plate with different cold deformations, annealing the steel plate which undergoes the cold deformation with heating rate controlled at 50-200 DEG C/s, with heating temperature within 750-950 DEG C and with heat preservation time within 5-100s, and cooling to the room temperature at a cooling rate of 50-400 DEG C/s to obtain a superfine austenite structure with micro-nano scale. The obdurability of the material is synchronously improved. The yield strength of the final product can be up to 750-800MPa, the strength of extension is up to 1100-1200MPa and the percentage of elongation is 35-45%.
Owner:UNIV OF SCI & TECH BEIJING

High-voltage lithium cobalt oxide cathode material for lithium-ion battery and preparation method of high-voltage lithium cobalt oxide cathode material

The invention discloses a high-voltage lithium cobalt oxide cathode material for a lithium-ion battery and a preparation method of the high-voltage lithium cobalt oxide cathode material. The high-voltage lithium cobalt oxide cathode material is prepared from a doped lithium cobalt oxide matrix and a coating on the surface of the doped lithium cobalt oxide matrix, wherein a general formula of the doped lithium cobalt oxide matrix is Li<x>Co<1-y>M<y>O<2-z>N<z>; the general formula of the coating is LiNi<x'>Co<y'>Al<z'>O<2>; and the preparation method comprises the following steps: firstly, obtaining the lithium cobalt oxide matrix Li<x>Co<1-y>M<y>O<2-z>N<z> through once sintering; secondly, preparing a lithium cobalt oxide cathode material precursor coated with Ni<x'>Co<y'>Al<z'>(OH)<2> on the surface by liquid-phase co-precipitation reaction; and finally obtaining the high-voltage lithium cobalt oxide cathode material through twice sintering. The high-voltage lithium cobalt oxide cathode material prepared by the method is good in processability and high in compaction density, has relatively high specific capacity and good cycle performance in a high-voltage state, and can be stably circulated at high voltage of 3.0V to 4.5V.
Owner:HUNAN CHANGYUAN LICO CO LTD +1

Method for preparing battery grade iron phosphate from waste and old lithium iron phosphate batteries

The invention discloses a method for preparing battery grade iron phosphate from waste and old lithium iron phosphate batteries and relates to the technical field of battery recovery. The method can prepare anhydrous battery grade iron phosphate by battery disassembly and separation, alkali leaching, acid leaching, oxidation, precipitation and calcination. Through alkali leaching and then acid leaching and precipitation, impurities such as aluminum in lithium iron phosphate can be removed and the purity of iron phosphate can be improved. The alkali leaching solution and the lithium-rich solution can be reused so that a recovery cost is reduced. After repeated acid supply, the lithium-rich solution immerses novel filter wastes so that the concentration of lithium in the solution and the recovery rate of lithium can be increased and the recovery cost of lithium can be reduced. pH at the precipitation end point is low in a range of 1.0-2.5 so that the formation trend of iron hydroxide isreduced. The aging process after the precipitation reaction can improve the purity of iron phosphate and the produced iron phosphate meets the industry standards. The whole process is carried out at alow temperature so that the corrosion of the solution to the equipment is delayed and the energy consumption and recycling cost are reduced.
Owner:INST OF RESOURCES UTILIZATION & RARE EARTH DEV GUANGDONG ACAD OF SCI
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