The invention discloses a preparation method and application of a bimetallic nano-
enzyme induced MOFs (at) CDs material, and the preparation method at least comprises the following steps: I, dissolving FeCl3, CoCl2 and 2-aminoterephthalic acid in N, N '-
dimethylformamide to form a
mixed solution I, and carrying out a reaction I to obtain a bimetallic MOFs material; step II, mixing tricarballylic acid and m-phenylenediamine, and carrying out a reaction II to obtain
carbon dot powder; step III, dissolving the
carbon dot powder obtained in the step II in
methanol, and adding
rhodamine B dye to obtain a CDs material; and IV, dissolving the bimetallic MOFs material obtained in the step I and the CDs material obtained in the step III in water, stirring, and
drying to obtain the MOFs (at) CDs material. The synthesized nano-
enzyme is simple to prepare and high in catalytic activity, the
carbon dot material is encapsulated into the MOFs material, the
fluorescence characteristic of the MOFs material is enhanced, and the carbon dot material is combined with o-phenylenediamine to be used for detecting H2O2.