The invention discloses a
nickel-
vanadium alloy target grain refinement method and an
equal channel angular extrusion die, and belongs to the field of
metal material
machining severe plastic deformation. The method comprises the steps that a
nickel-
vanadium cast
ingot is subjected to homogenizing annealing (1200 DEG C / 2 h, AC), then 8-pass
extrusion is conducted through a BC path, and the total deformation is 165%. Each pass of
extrusion is divided into three stages, the
extrusion rates of the first four passes are the same, and the extrusion rates of the last four passes are relatively slow. The extrusion rate of each pass in the first four passes of extrusion is 10mm / s, 8mm / s and 6mm / s, and the extrusion rate of each pass in the last four passes of extrusion is 8mm / s, 6mm / s and 4mm / s. The
equal channel angular extrusion die is composed of an L-shaped channel, the inner angle of the die is 120 degrees, and the outer angle of the die is 30 degrees. Then
stress relief annealing (700 DEG C / 1 h, AC) is carried out; then large-deformation cold rolling is carried out, the deformation is 90%, and a sample is thinned to 3 mm; and then the plate is subjected to recrystallization annealing (550-850 DEG C / 1 h, AC). Compared with the prior art, the obtained structure is compact and has few defects, the structure is uniform,
crystal grains are fine, and the strength is improved.