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34results about "Esters preparation by oligomerisation" patented technology

Polycondensation Catalyst for Producing Polyester and Method for Producing Polyester Using the Same

The invention provides a polycondensation catalyst for producing polyester by an esterification reaction or a transesterification reaction between a dicarboxylic acid or ester-forming derivative thereof and a glycol, wherein the polycondensation catalyst comprises particles of a solid base having on their surfaces either a coat layer of titanic acid in an amount of from 0.1 to 50 parts by weight in terms of TiO2 per 100 parts by weight of the solid base, or an inner coat layer of an oxide of at least one element selected from silicon, aluminum and zirconium or a composite oxide of at least two elements selected from silicon, aluminum and zirconium in an amount of from 1 to 20 parts by weight per 100 parts by weight of the solid base and an outer coat layer of titanic acid in an amount of from 0.1 to 50 parts by weight in terms of TiO2 per 100 parts by weight of the solid base
Owner:SAKAI CHEM IND CO LTD

Modified acrylic acid oligomer and dirt-resisting paint containing the oligomer

InactiveCN101245005AGood and long-lasting anti-fouling effectApplicable radiation curing mechanismAntifouling/underwater paintsPaints with biocidesPolyesterOligomer
The invention provides a modified acrylic acid oligomer, which comprises polymerizing units derived from the following monomers, (1) acrylic monomers, (2) monomers of fluoride acrylic monomers, silicone monomers or the mixture of the two, and (3) three-grade carboxylic ester monomers which depend; wherein, the oligomer also comprises groups of modifier which consists of epoxy acrylate, amidine formic ester acrylate, polyester acrylate, methacrylic 2-hydroxyethyl ester and the mixture; the modified acrylic acid oligomer also provides an antipollution coating containing the modified acrylic acid oligomer.
Owner:ETERNAL MATERIALS CO LTD

Synthetic method of brush type homopolymer and copolymer containing conjugate oligomeric branched chains

The invention discloses a synthetic method of a brush type homopolymer and a brush type copolymer containing conjugate oligomeric branched chains. In the synthesis process of a novel monomer, a metal catalysis coupling reaction and an esterification reaction are adopted, so that conjugate alkene monomers such as oligo-containing polyfluorene, oligomeric benzene, oligomeric benzyne, oligomeric carbazole, oligomeric thiophene and the like are synthesized; and a way for grafting and grafting to is adopted, and radical polymerization (including atom transfer radical polymerization) are performed, so that a series of brush type homopolymers and copolymers with conjugate branched chains are obtained, homopolymerization, binary irregular copolymerization and block copolymerization, and ternary irregular copolymerization and block copolymerization of a monomer containing a conjugate branched chain are realized, and special brush type homopolymers and brush type copolymers are obtained. The synthetic method disclosed by the invention is simple, convenient and practicable; a synthesized brush type polymer has a controllable structure; and a three-dimensional structural design of a large molecular strain is realized, and combination of a conjugate structure and a brush type structure is realized, so that a polymer with excellent comprehensive performance is obtained.
Owner:GUILIN UNIVERSITY OF TECHNOLOGY

Methods of reproducing lactic acid components by using lactic acid based by-products

A lactic acid based by-product formed in a process of producing a lactic acid based composition is subjected to racemization in the presence or absence of a catalyst to thereby obtain a lactic acid component having substantially optical inactivity. Then, lactide or polylactic acid having optical inactivity can be obtained from the lactic acid component having the optical inactivity. The obtained lactide or polylactic acid is mixed with lactide or polylactic acid having an optical purity in a range of 90 to 100% e.e. at a predetermined ratio to thereby obtain lactide or polylactic acid having a desired optical purity.
Owner:TEIJIN LTD

Catalytic processes for preparing estolide base oils

Provided herein are processes for preparing estolides and estolide base oils from fatty acid reactants utilizing catalysts. Further provided herein are processes for preparing carboxylic esters from at least one carboxylic acid reactant and at least one olefin.
Owner:BIOSYNTHETIC TECH

Fuel and base oil blendstocks from a single feedstock

A method comprising providing a fatty acyl mixture comprising: (i) a C10-C16 acyl carbon atom chain content of at least 30 wt. % wherein at least 80% of the C10-C16 acyl carbon atom chains are saturated; and (ii) a C18-C22 acyl carbon atom chain content of at least 20 wt. % wherein at least 50% of the acyl C18-C22 carbon atom chains contain at least one double bond; hydrolyzing the mixture to yield a quantity of C10-C16 saturated fatty acids and C18-C22 unsaturated fatty acids; oligomerizing at least some of the C18-C22 unsaturated fatty acids to yield a quantity of C36+ fatty acid oligomers; hydrotreating at least some of the C10-C16 saturated fatty acids and at least some of the C36+ fatty acid oligomers to yield a quantity of diesel fuel blendstock and C36+ alkanes; and separating at least some of the diesel fuel blendstock from the C36+ alkanes.
Owner:CHEVROU USA INC

Preparation method of conjugated diene and polar monomer segmented copolymer with low molecular weight

A preparation method of a conjugated diene and polar monomer segmented copolymer with low molecular weight belongs to the field of copolymer synthesis. The method can solve the problem that the existing conjugated diene and polar monomer copolymer is high in molecular weight and preparation cost. The method comprises the steps of adding a reaction monomer and a catalyst to an alkane solvent according to the molar ratio of (100-2000):1 for reaction to obtain a solution a, adding the polar monomer to the obtained solution a to obtain a solution b, adding alcohol solution to the obtained solution b with the molar ratio of the polar monomer to the catalyst of (10-800):1, and condensing the conjugated diene and polar monomer segmented copolymer. For the synthesized conjugated diene and polar monomer segmented copolymer, the number-average molecular weight is 1.2*10<3>-25.0*10<3>, and the molecular weight distribution is 1.20-1.50.
Owner:CHANGCHUN INST OF APPLIED CHEMISTRY - CHINESE ACAD OF SCI

Sheet catalyst for synthesis of dimmer acid ester and preparation method thereof

A novel flaky catalyst for synthesizing a dimmer acid ester consists of activated clay, a promoter and an adhesive pore-forming agent, wherein the activated clay accounts for 65-85 percent, the promoter accounts for 2-10 percent, and the adhesive pore-forming agent accounts for 13-25 percent. The preparation method for the catalyst comprises the following steps of: preparing the powder of the activated clay with a particle size of 150-250 meshes; mixing the raw materials evenly according to the partition ratio; tabletting and forming; drying the mixture at 105 DEG C; calcining the mixture at 300-400 DEG C; and cooling down and packaging the mixture. The method is simple and feasible. The catalyst which has good activity and high strength is easy to be separated from products with less products carried. In addition, the catalyst is easy to be regenerated.
Owner:溧阳常大技术转移中心有限公司

Fuel and base oil blendstocks from a single feedstock

A method comprising providing a fatty acyl mixture comprising: (i) a C10-C16 acyl carbon atom chain content of at least 30 wt. % wherein at least 80% of the C10-C16 acyl carbon atom chains are saturated; and (ii) a C18-C22 acyl carbon atom chain content of at least 20 wt. % wherein at least 50% of the acyl C18-C22 carbon atom chains contain at least one double bond; hydrolyzing the mixture to yield a quantity of C10-C16 saturated fatty acids and C18-C22 unsaturated fatty acids; oligomerizing at least some of the C18-C22 unsaturated fatty acids to yield a quantity of C36+ fatty acid oligomers; hydrotreating at least some of the C10-C16 saturated fatty acids and at least some of the C36+ fatty acid oligomers to yield a quantity of diesel fuel blendstock and C36+ alkanes; and separating at least some of the diesel fuel blendstock from the C36+ alkanes.
Owner:CHEVROU USA INC

Lactate Production Process

A process for producing alkyl R-lactate from an initial compound comprising substructure (I) is provided. The process involves producing an intermediate comprising R,R- and S,S-lactide from the initial compound, wherein the initial compound is subjected to stereoisomerisation conditions; and reacting at least a portion of the intermediate with an alkyl alcohol to produce a product comprising alkyl R-lactate, wherein alkyl R-lactate is produced in the presence of an enzyme. Also provided are processes for the production of R-lactic acid, oligomeric R-lactic acid, R,R-lactide, poly-R-lactic acid and stereocomplex lactic acid.
Owner:NATUREWORKS LLC

Macromolecule for delivering protein, polypeptide or peptide drugs and a production method for the same, and a slow release composition for protein, polypeptide or peptide drugs and a production method for the same

The present invention relates to a macromolecule for delivering protein, polypeptide or peptide drugs and to a production method for the same, as well as to a slow release composition for protein, polypeptide or peptide drugs comprising the same, and more specifically relates to a polylactic acid derivative compound of Chemical formula 1 of which the numerical average molecular weight is no more than 7000 daltons and to a production method for the same, as well as to a slow release composition for protein, polypeptide or peptide drugs using the same and to a production method for the same.
Owner:SAMYANG HLDG CORP

Method for producing multisubstituted biphenyl compound and solid catalyst to be used therein

A method for producing a multisubstituted biphenyl compound represented by general formula (2), said method comprising a step for coupling a substituted benzene compound represented by general formula (1) in the presence of a solid catalyst wherein gold is fixed on a support.
Owner:KYUSHU UNIV +1

Method for producing compound

A method is provided for producing a compound, including a step of mixing a compound (1) having one or two leaving groups, a compound (2) having one or two boron atom-containing leaving groups, an organic base (P), and at least one selected from a phase transfer catalyst and an organic base (Q) larger in the number of carbon atoms than the above-mentioned organic base in the presence of a transition metal catalyst. The method thereby performs a coupling reaction between the above-mentioned compound (1) and the above-mentioned compound (2).
Owner:SUMITOMO CHEM CO LTD

Hydroxyl-terminated polyacrylate oligomer as well as preparation method and application thereof

The invention relates to a preparation method of hydroxyl-terminated polyacrylate oligomers, which comprises the following steps: preparing low molecular weight polyacrylate oligomers with controllable molecular weight, such as polybutylacrylate, polyethylacrylate, oly(isooctyl acrylate), polymethyl methacrylate, a block copolymer of butyl acrylate and methyl methacrylate, a block copolymer of themethyl methacrylate and dimethylaminoethyl methacrylate, and the like by adopting atom transfer radical polymerization (ATRP) and using organic halide as an initiating agent; and then carrying out terminal group modification on the polymers by N-methylethanolamine to obtain the hydroxyl-terminated polyacrylate oligomers with controllable molecular weight. The prepared hydroxyl-terminated polyacrylate oligomers can be used for the production of polyurethane. Because the molecular weight of the hydroxyl-terminated polyacrylate oligomers is controllable, a polyurethane material with special performance can be prepared.
Owner:溧阳常大技术转移中心有限公司

Synthetic method of brush type homopolymer and copolymer containing conjugate oligomeric branched chains

The invention discloses a synthetic method of a brush type homopolymer and a brush type copolymer containing conjugate oligomeric branched chains. In the synthesis process of a novel monomer, a metal catalysis coupling reaction and an esterification reaction are adopted, so that conjugate alkene monomers such as oligo-containing polyfluorene, oligomeric benzene, oligomeric benzyne, oligomeric carbazole, oligomeric thiophene and the like are synthesized; and a way for grafting and grafting to is adopted, and radical polymerization (including atom transfer radical polymerization) are performed, so that a series of brush type homopolymers and copolymers with conjugate branched chains are obtained, homopolymerization, binary irregular copolymerization and block copolymerization, and ternary irregular copolymerization and block copolymerization of a monomer containing a conjugate branched chain are realized, and special brush type homopolymers and brush type copolymers are obtained. The synthetic method disclosed by the invention is simple, convenient and practicable; a synthesized brush type polymer has a controllable structure; and a three-dimensional structural design of a large molecular strain is realized, and combination of a conjugate structure and a brush type structure is realized, so that a polymer with excellent comprehensive performance is obtained.
Owner:GUILIN UNIVERSITY OF TECHNOLOGY

Production method of polysubstituted biphenyl compound and solid catalyst used in the production method

The present invention is a method for producing a polysubstituted biphenyl compound represented by the following general formula (2), which comprises making the substituted benzene represented by the following general formula (1) Steps for compound coupling.
Owner:KYUSHU UNIV +1

(METH)acrylic oligomers

The invention provides (meth)acrylic oligomers prepared from C1-C20 alkyl and C5-C20 cycloalkyl (meth)acrylates, wherein said oligomers have a Mn of about 300 g / mole to about 3,000 g / mole; a Mw of about 700 g / mole to about 6,000 g / mole; a Mz of about 900 g / mole to about 10,000 g / mole. The oligomers may have a Yellowness Index, according to ASTM E313 of less than 2. The oligomers of the invention are useful as tackifiers in adhesive compositions, but also are believed to be useful also in general polymer modification as plasticizers, leveling agents, viscosity reducers (i.e., rheology modifiers), and for increasing solids content in solvent-borne applications of all types with little detrimental impact on viscosity. The invention also provides adhesive compositions and laminate articles coated on at least one side with the adhesive compositions of the invention.
Owner:SYNTHOMER ADHESIVE TECH LLC

Mandelic acid condensation polymers

Disclosed herein are compounds and compositions useful for reducing the risk of infection. In particular, disclosed herein are mandelic acid condensation polymers, compositions comprising such compounds, processes for producing such compounds, and methods of using such compounds.
Owner:RUSH UNIV MEDICAL CENT +1

Novel intermediate compound for manufacturing bixin ethyl ester and method of manufacturing the same

The present invention relates to a method of manufacturing norbixin or bixin ethyl ester, which is a carotenoid-based compound, from a novel intermediate compound. When the novel intermediate compound is used, it is possible to manufacture norbixin or bixin ethyl ester in high yield through a simple process.
Owner:MYONGJI UNIV IND & ACAD COOPERATION FOUND

Process to prepare a cyclic oligomer and a cyclic oligomer obtainable thereby and a process to polymerize it

A process to prepare a (iv) cyclic polyester oligomer composition includes a cyclic polyester oligomer having furanic units and two to five repeat units. The process includes (a) reacting a monomer composition including: (i) a bifunctional furan-derivative and (ii) a diol in an linear oligomerization step to produce a (iii) linear oligomer composition including a linear oligomer species, (b) reacting the (iii) linear oligomer composition in a distillation-assisted cyclization (DA-C) step to form a (iv) cyclic polyester oligomer composition and a (v) diol byproduct. The (v) diol byproduct is removed by evaporation in the distillation-assisted cyclization (DA-C) step.
Owner:SULZER MANAGEMENT AG
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