The application discloses a kind of equipment and method for preparing MOFs by
plasma assisted flash
joule heat, the equipment includes central
control system, vacuum
system, gas inlet
system,
signal acquisition
system, power supply system, tubular reaction device;Central
control system is used for the instruction of equipment each area to issue and control;Vacuum system is used to control the vacuum degree required by reaction, and is monitored in real time by vacuum gauge;Gas inlet system is used to provide the
atmosphere required by reaction;
Signal acquisition system acquires temperature,
voltage, current in real time during reaction, input to central
control system;Power supply system provides electrical energy for tubular lifting reaction device;Tubular reaction device fixed substrate and precursor solution on substrate and generates
plasma, realize the uninterrupted performance of
plasma processing and flash
joule heat processing.This equipment realizes the uninterrupted performance of plasma-
joule heat, can realize the rapid preparation of MOFs, significantly improve the problem of long cycle,
high energy consumption of traditional preparation method such as hydrothermal method, solvothermal method.