Liquid crystal sealing agent and liquid crystal display cell using the same
A kind of liquid crystal display unit, liquid crystal sealing agent technology
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Embodiment 1
[0064] 75 parts by weight of epoxy acrylate resin KAYARAD R-94220 (produced by Nippon Kayaku Co., Ltd.; bisphenol F epoxy resin of epoxy acrylate), 25 parts by weight of epoxy resin RE-203 (produced by Nippon Kayaku Co. ., Ltd. production; Epoxy equivalent is 233 grams / equivalent, the bisphenol S type epoxy resin of ethylene oxide-addition), 5 parts by weight photoinitiator KAYACURE RPI-4 (by Nippon Kayaku Co., Ltd. ( NipponKayaku Co., Ltd.) production; 2-isocyanatoethylacrylate methyl ester and 2-hydroxy-1-[4-(2-hydroxyethoxy)phenyl]-2-methylpropan-1-one reaction product) and 1.5 parts by weight of a silane coupling agent Sila-Ace S-510 (produced by Chisso Corp.; 3-glycidoxypropyltrimethoxysilane) were mixed to obtain a resin solution . Then, using a ball mill, 17.5 parts by weight of Nanotec Alumina SPC (manufactured by CI Kasei Co., Ltd.; spherical alumina with an average particle size of 50 nm) was used as a filler and 3 parts by weight of butadiene-formazine Alkyl acryl...
Embodiment 2
[0066] With 75 parts by weight of epoxy acrylate resin KAYARAD R-94220 (produced by Nippon Kayaku Co., Ltd.; bisphenol F epoxy resin of epoxy acrylate), 25 parts by weight of epoxy resin RE-203 (by Nippon Kayaku Co., Ltd. Company production; Epoxy equivalent is 233 grams / equivalent, the bisphenol S type epoxy resin of oxirane-addition), 5 weight parts photoinitiators KAYACURE RPI-4 (produced by Nippon Kayaku Co., Ltd.; 2- The reaction product of methyl isocyanatoethacrylate and 2-hydroxy-1-[4-(2-hydroxyethoxy) phenyl]-2-methylpropan-1-one) and 1.5 parts by weight of silane coupling Sila-Ace S-510 (manufactured by Chisso Corp.; 3-glycidoxypropyltrimethoxysilane) was mixed to obtain a resin solution. Then, using a ball mill, 17.5 parts by weight of Nanotec Alumina SPC (manufactured by CI Chemical Industry Co., Ltd.; spherical alumina with an average particle size of 50 nm) as a filler and 3 parts by weight of butadiene-alkylmethacrylate-styrene copolymerized A substance (produc...
Embodiment 3
[0068] With 75 parts by weight of epoxy acrylate resin KAYARAD R-94220 (produced by Nippon Kayaku Co., Ltd.; bisphenol F epoxy resin of epoxy acrylate), 25 parts by weight of epoxy resin RE-203 (by Nippon Kayaku Co., Ltd. Company production; Epoxy equivalent is 233 grams / equivalent, the bisphenol S type epoxy resin of oxirane-addition), 5 weight parts photoinitiators KAYACURE RPI-4 (produced by Nippon Kayaku Co., Ltd.; 2- The reaction product of methyl isocyanatoethacrylate and 2-hydroxy-1-[4-(2-hydroxyethoxy) phenyl]-2-methylpropan-1-one) and 1.5 parts by weight of silane coupling Sila-Ace S-510 (manufactured by Chisso Corp.; 3-glycidoxypropyltrimethoxysilane) was mixed to obtain a resin solution. Then, using a ball mill, 17.5 parts by weight of Nanotec Alumina SPC (manufactured by CI Chemical Industry Co., Ltd.; spherical alumina with an average particle size of 50 nm) as a filler and 3 parts by weight of butadiene-alkylmethacrylate-styrene copolymerized A substance (produc...
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