Identification method of precious rosewood based on chemical fingerprint
A technology of fingerprints and chemical fingerprints, applied in scientific instruments, measuring devices, instruments, etc., can solve problems such as subjective uncertainty, great difference in function and value, time-consuming and labor-intensive problems, and achieve accurate and reliable results
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[0044] 1 Obtain fingerprints of standard samples and unknown samples
[0045] 1.1 Sample pretreatment
[0046] A. cut 4 kinds of standard mahogany samples and 2 kinds of unknown mahogany heartwood samples as embodiments into thin slices with a carving knife, weigh 1.0g in a 50ml Erlenmeyer flask with a stopper;
[0047] b. Add 20ml of absolute ethanol, ultrasonically extract for 25 minutes and then filter, add 20ml of absolute ethanol to the filter residue, ultrasonically extract again for 25min and then filter, combine the two filtrates as the stock solution;
[0048] c. Take 10ml of the stock solution in a sample bottle, and concentrate to remove all solvents by nitrogen blowing;
[0049] d. Add 1 ml of absolute ethanol, filter through an organic phase microporous membrane (0.45 μm), and place in a 2 ml standard sample bottle.
[0050] 1.2 Acquisition of gas chromatography (GC-FID) fingerprints
[0051] The GC-FID parameters were set as follows:
[0052] Injector Tempera...
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