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Method for performing surface modification of polyester filaments by remote plasmas

A remote plasma and surface modification technology, applied in the field of ion one-step surface modification, can solve problems such as material performance degradation, and achieve the effect of short processing time and wide range

Active Publication Date: 2013-05-22
JIANGSU HENGLI CHEM FIBER
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, when using these conventional plasmas to treat materials, because the plasma conditions are significantly affected by changes in electric field strength and pressure, the electron energy in the plasma has a wide distribution and contains some high-energy particles, which will cause plasma dissociation and make the material properties Deterioration occurs

Method used

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  • Method for performing surface modification of polyester filaments by remote plasmas
  • Method for performing surface modification of polyester filaments by remote plasmas

Examples

Experimental program
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Effect test

Embodiment 1

[0031] Place the polyester FDY fiber with a circular cross-section of 73dtex / 192f in the downstream direction of the airflow 5cm away from the plasma discharge area, and pump the plasma to a vacuum of 1×10 -2 Pa, with oxygen as the carrier gas, sulfur dioxide as the modified gas, and oxygen / sulfur dioxide as a mixed gas into the plasma, the volume content of sulfur dioxide is 10%, the gas pressure is 5Pa, and the discharge power is 100W. After 5s discharge treatment, it is obtained Sulfonic acid modified fiber.

Embodiment 2

[0033] Place the polyester FDY fiber with a circular cross-section of 73dtex / 192f in the downstream direction of the airflow 60cm away from the plasma discharge area, and pump the plasma to a vacuum of 5×10 -2 Pa, with oxygen as the carrier gas, sulfur dioxide as the modified gas, and oxygen / sulfur dioxide as a mixed gas into the plasma, the volume content of sulfur dioxide is 90%, the gas pressure is 100Pa, and the discharge power is 100W. After 120s discharge treatment, it is obtained Sulfonic acid modified fiber.

Embodiment 3

[0035] Place the polyester FDY fiber with a circular cross-section of 73dtex / 192f in the downstream direction of the airflow 10cm away from the plasma discharge area, and pump the plasma to a vacuum of 1×10 -2 Pa, with oxygen as the carrier gas, sulfur dioxide as the modified gas, and oxygen / sulfur dioxide as a mixed gas into the plasma, the volume content of sulfur dioxide is 50%, the gas pressure is 30Pa, and the discharge power is 20W. After 30s discharge treatment, it is obtained Sulfonic acid modified fiber.

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Abstract

The invention relates to a method for performing the surface modification of polyester fiber materials, in particular to a method for performing the surface modification of polyester filaments by remote plasmas. The method comprises the following steps of: vacuumizing plasma equipment, introducing sulfur dioxide and oxygen in a reasonable volume ratio into the plasma equipment simultaneously, anddischarging to generate the plasmas under the action of an electric field, wherein the generated plasmas react on the surfaces of the materials to be modified to achieve the effect of modification. The method is characterized in that the modified polyester filaments are put in the downstream along the direction of airflow and have a certain distance away from a plasma discharging area. Aiming at the problem of the conventional plasmas in the process of the surface treatment of the polyester fibers, for example, the performance of fiber materials is deteriorated due to the bombardment of high-energy particles on the surfaces of the fiber materials in modifying, so the treatment method of the remote plasmas is provided. The surfaces of the materials are modified by the treatment of the remote plasmas, and other performance keeps stable basically.

Description

technical field [0001] The invention relates to a method for surface modification of polyester fiber materials, in particular to a method for remote plasma surface modification of polyester long fibers, specifically a remote plasma one-step surface modification method for polyester long fibers sexual method. Background technique [0002] Plasma is the fourth state of matter, which is composed of a large number of electrons, cations, and free radicals. These microscopic particles with high activity and high energy can interact with the surface of the material, thereby endowing the material without changing the bulk properties of the material. With new properties, such as adhesion, reactivity, biocompatibility, water absorption, etc., the field of use of materials can be greatly expanded. At present, low-temperature plasma modification is commonly used in the field of material modification. Usually, under vacuum conditions, capacitive or inductive excitation is used to genera...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06M10/06
Inventor 沈风雷丁建中陈国强汤方明王丽丽
Owner JIANGSU HENGLI CHEM FIBER
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