Zn2(VO4)(IO3) and preparation method and application thereof
A technology of VO4 and unit cell volume, applied in optics, instruments, nonlinear optics, etc.
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[0014] Synthesis of compound Zn by hydrothermal synthesis 2 (VO 4 )(IO 3 )
[0015] Zn(CH 3 COO) 2 ·2H 2 O (0.5 mmol, 110 mg), V 2 O 5 (0.11 mmol, 20 mg), I 2 O 5 (0.92 mmol, 310 mg) and H 2 O (2ml) was put into the hydrothermal reaction kettle and mixed uniformly, sealed, placed in a box-type resistance furnace, heated from 30°C to 190°C after 600 minutes, reacted at a constant temperature for 5760 minutes, and finally dropped to 50°C every hour at 3°C , Can get colorless flake crystals.
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