Method for preparing 2, 6-dichlorobenzonitrile
A technology of dichlorobenzonitrile and dichlorotoluene, which is applied in the production field of chemically synthesizing 2,6-dichlorobenzonitrile, can solve the problems of not being able to meet market demand, difficult production control, high cost, etc., and reduce the generation of solid waste , Low production cost, less raw material consumption
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[0020] Production steps:
[0021] 1. First add 750kg of 2,6-dichlorotoluene and 3-15kg of phosphorus pentachloride into the reactor, then turn on the light source (luminous flux of 50000-500000lm, color temperature of 1000-6000k), and pass high-temperature steam into the jacket , so that the temperature in the reactor reaches 80-120°C, and at the same time, chlorine gas is introduced at a ventilation rate of 25-40kg / h. Chlorine gas is passed through at a ventilation rate of 80 kg / h, and after 0.5 to 2 hours, chlorine gas is passed through at a ventilation rate of 40 to 50 kg / h, and the reaction is kept warm until the reaction is completed.
[0022] Shut off the chlorine gas, absorb the generated hydrogen chloride gas, and absorb it with water to generate hydrochloric acid, which can be sold as a by-product.
[0023] By passing low-temperature water into the jacket, the pressure in the reaction kettle is controlled to reduce to a slight negative pressure and 50-70°C, and then ...
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