Preparation method of Jinma Gantai preparation for treating hepatitis
A technology for Jinmagantai and preparations, which is applied in the field of preparation of Jinmagantai preparations, can solve the problems of simple and rough methods, affecting the curative effect, and low content of active ingredients.
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Embodiment 1
[0032] Example 1: 288.2g of horseshoe gold, 153.3g of iron clad gold, 115g of verbena, 191.6g of Fangji, 115g of Patrinia, 153.3g of Epimedium, 153.3g of Astragalus, 153.3g of Radix Paeoniae Rubra, 230g of Salvia miltiorrhiza
[0033] Add the above nine medicinal materials, add 6 times of water and decoct twice, 1.5 hours each time, combine the decoction, filter, and concentrate the filtrate to a clear paste with a relative density of 1.14-1.16 (70-75°C), cool to room temperature, add Extract twice with the same amount of n-butanol, combine the n-butanol solution, add hydrochloric acid to the water solution to adjust the pH to 3-4, add the same amount of n-butanol to extract twice, combine the n-butanol solution, and adjust the pH of the water solution to 9 with ammonia water ~10, add the same amount of n-butanol to extract twice, combine all the n-butanol liquids, recover the solvent under reduced pressure to a thick paste with a relative density of 1.34~1.40 (50~60°C), add 4 ...
Embodiment 2
[0034] Example 2: 288.2g of horseshoe gold, 153.3g of iron-coated gold, 115g of verbena, 191.6g of Fangji, 115g of Patrinia, 153.3g of Epimedium, 153.3g of Astragalus, 153.3g of Radix Paeoniae Rubra, 230g of Salvia miltiorrhiza
[0035]Add the above nine medicinal materials, add 6 times of water and decoct twice, 1.5 hours each time, combine the decoction, filter, and concentrate the filtrate to a clear paste with a relative density of 1.14-1.16 (70-75°C), cool to room temperature, add Extract twice with the same amount of n-butanol, combine the n-butanol solution, add hydrochloric acid to the water solution to adjust the pH to 3-4, add the same amount of n-butanol to extract twice, combine the n-butanol solution, and adjust the pH of the water solution to 9 with ammonia water ~10, add the same amount of n-butanol to extract twice, combine all n-butanol liquids, recover the solvent under reduced pressure to a thick paste with a relative density of 1.34~1.40 (50~60°C), dry under...
Embodiment 3
[0036] Example 3: 288.2g of horseshoe gold, 153.3g of iron-coated gold, 115g of verbena, 191.6g of Fangji, 115g of Patrinia, 153.3g of Epimedium, 153.3g of Radix Astragali, 153.3g of Radix Paeoniae Rubra, 230g of Salvia miltiorrhiza
[0037] Add the above nine medicinal materials, add 6 times of water and decoct twice, 1.5 hours each time, combine the decoction, filter, and concentrate the filtrate to a clear paste with a relative density of 1.14-1.16 (70-75°C), cool to room temperature, add Extract twice with the same amount of n-butanol, combine the n-butanol solution, add hydrochloric acid to the water solution to adjust the pH to 3-4, add the same amount of n-butanol to extract twice, combine the n-butanol solution, and adjust the pH of the water solution to 9 with ammonia water ~10, adding an equal amount of n-butanol for extraction twice, combining all the n-butanol liquids, recovering the solvent under reduced pressure to a thick paste with a relative density of 1.34~1.4...
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