Navy blue or black disperse dye composition
A technology of disperse dyes and compositions, applied in organic dyes, dyeing methods, textiles and papermaking, etc., can solve the problems of lack of washing fastness and sublimation fastness
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Embodiment 1
[0093] The former dye A1 shown in formula (I) gets 2 grams, A18 gets 8 grams, the former dye B1 shown in formula (II) gets 5 grams, B30 gets 7.5 grams, the former dye C6 shown in formula (III) gets 12.5 grams, the former dyestuff D3 shown in formula (IV) gets 15 grams, then adds 67 grams of dispersant MF, 8 grams of sodium lignin sulfonate, 153 grams of water and carries out dispersion treatment together with sand mill, then spray drying, to obtain final product Dye compositions of the invention.
Embodiment 2~27
[0095] According to the preparation method of Example 1, according to the data shown in Table 5, at least one dye A, at least one dye B, at least one dye C, at least one dye D and dispersant MF, sodium lignosulfonate Blending with water, sand milling to disperse, and spray drying to obtain finished disperse dyes. Among them, the structural formulas defined by the substituents of the dyes A, B, C, and D are shown in Tables 1 to 4.
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Embodiment 28
[0107] Take 2.5 grams of the disperse dyes prepared in Examples 1-27 and disperse them in 500 milliliters of water to form a dye suspension, draw 20 milliliters and mix them with 80 milliliters of water, adjust the pH of the dyeing bath to 4-5 with acetic acid, and heat up to 70 °C At the same time, put 5 grams of polyester fiber cloth for dyeing, heat up from 70°C to 130°C within 30 minutes, keep warm for 50 minutes, cool to below 90°C, drain and wash. Then put the cloth sample into 100 milliliters of reduction cleaning solution containing 1 gram per liter of caustic soda and 3 grams per liter of sodium hydrosulfite to clean at 80° C. for 20 minutes. According to the national standard GB / T2397-2003, the lifting power of the disperse dyes prepared in Examples 1 to 27 was measured, and the national standard GB / T3921-2008, GB / T3920-2008, GB / T8427-2008, GB / T5718-1997 were used to test their resistance Washing, rubbing, light fastness and sublimation color fastness. The test resu...
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