Underwater gas chromatography system for realizing in-situ test for H2 and CH4 in seawater and operation method thereof

A gas chromatography system and in-situ testing technology, which can be applied to measurement devices, instruments, scientific instruments, etc., and can solve the problem that gas chromatography technology does not realize underwater in-situ detection.

Inactive Publication Date: 2016-05-18
TONGJI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] Judging from the current testing methods of deep-sea gas, most of them use shipboard system sampling and then analysis. At present, there are few devices that can detect gas in situ in the deep-sea high-pressure environment, and some sensor technologies are more mature. As a gas An important means of testing - gas chromatography technology has not yet achieved underwater in-situ detection

Method used

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  • Underwater gas chromatography system for realizing in-situ test for H2 and CH4 in seawater and operation method thereof
  • Underwater gas chromatography system for realizing in-situ test for H2 and CH4 in seawater and operation method thereof
  • Underwater gas chromatography system for realizing in-situ test for H2 and CH4 in seawater and operation method thereof

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Embodiment 1

[0031] Such as figure 1 As shown, the underwater gas chromatography system is composed of three major parts, seawater automatic sampling and gas membrane extraction unit, multi-component gas automatic detection and self-calibration unit, exhaust gas recovery unit. Among them, the multi-component gas automatic detection and self-calibration unit, and the exhaust gas recovery unit are all packaged in the high-pressure sealed instrument cabin, and the seawater automatic sampling and gas film extraction unit are installed on the end cover of the instrument cabin.

[0032] The automatic seawater sampling and gas membrane extraction unit consists of an inlet filter 1, a membrane sampling device, a water pump 3, and an outlet filter 4, wherein the membrane sampling device includes a seawater sample chamber 2, a semipermeable membrane 5, and a gas chamber 6.

[0033] The multi-component gas automatic detection and self-calibration unit packaged in a high-pressure sealed instrument com...

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Abstract

The invention relates to an underwater gas chromatography system for realizing in-situ test for H2 and CH4 in seawater and an operation method thereof. The underwater gas chromatography system comprises a seawater automatic sampling and gas membrane extracting unit, a multi-component gas automatic detecting and self-correcting unit and an exhaust gas recovering unit, wherein the seawater automatic sampling and gas membrane extracting unit is mounted on an instrument cabin end cover; the multi-component gas automatic detecting and self-correcting unit and the exhaust gas recovering unit are packaged in a high-pressure sealing instrument cabin; the seawater automatic sampling and gas membrane extracting unit is used for separating and extracting gas from a seawater sample and the gas is applied to the subsequent assay determination of a gas automatic detection device; the multi-component gas automatic detecting and self-correcting unit is used for quantitatively analyzing and determining the content of the gas in the seawater by using a pulse helium ionization detector; the exhaust gas recovering unit is used for storing the exhaust gas discharged from the system in an exhaust gas bottle, keeping the system pressure within a suitable numerical range and ensuring the normal running of all functional components in the system. According to the invention, the gas chromatographic technique is applied to underwater position and can be used for performing underwater accurate in-situ test on various dissolvable gases in deep sea and truly reflecting the content of the in-situ gases on seabed.

Description

technical field [0001] The invention belongs to the technical field of gas chromatographic analysis, in particular to a method capable of realizing H in seawater 2 、CH 4 An underwater gas chromatography system for in-situ testing of other gases and its operating method. Background technique [0002] Submarine hydrothermal activities will eject a large amount of CH 4 、H 2 , CO 2 and other gases, the disturbed decomposition of natural gas hydrate will also release a large amount of CH 4 and other hydrocarbon gases, resulting in abnormally high content distribution of these tracer gases in seawater. By quickly detecting and tracking the abnormal distribution characteristics of these tracer gases, it can provide a fast and effective scientific basis for finding and reasonably evaluating resources such as seabed hydrothermal sulfides and gas hydrates. At the same time, CH in the ocean 4 、H 2 and CO 2 Gas and other gases are also an important source of energy for organism...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/02
CPCG01N30/02G01N2030/025
Inventor 杨群慧季福武王虎米智楠周怀阳金璐韦婧
Owner TONGJI UNIV
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