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Magnesium diffusion preparation method for magnesium diboride superconducting wire rod based on MgB<4> precursor powder

A technology of magnesium diboride and superconducting wire, which is applied in the usage of superconductor elements, cable/conductor manufacturing, superconductive devices, etc. High density, high density, and the effect of increasing the filling rate of superconducting phase

Active Publication Date: 2016-11-16
INST OF ELECTRICAL ENG CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the disadvantage of this method is that after the central magnesium rod diffuses into the boron layer, a large area of ​​holes will be formed in the original center of the magnesium rod, and the filling rate of the superconducting phase is lower than 5%, which makes its engineering critical current density significantly larger. decline, and this process is in the preparation of MgB 2 Wire is still immature

Method used

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  • Magnesium diffusion preparation method for magnesium diboride superconducting wire rod based on MgB&lt;4&gt; precursor powder
  • Magnesium diffusion preparation method for magnesium diboride superconducting wire rod based on MgB&lt;4&gt; precursor powder
  • Magnesium diffusion preparation method for magnesium diboride superconducting wire rod based on MgB&lt;4&gt; precursor powder

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Experimental program
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Effect test

Embodiment 1

[0030] Step 1. According to MgB 2 MgB in wire preparation process 4 Magnesium, boron and carbon molar ratios required for powder generation Weigh magnesium powder, amorphous boron powder and nano-carbon powder into a ball mill and mix them, and then mix them according to MgB 2 MgB in wire preparation process 4 The mass ratio of raw materials and grinding balls required for powder generation is put into the grinding balls, and finally the ball mill tank containing the raw materials and grinding balls is sealed and fixed to the planetary ball mill, according to MgB 2 MgB in wire preparation process 4 The ball milling rate and ball milling time required for powder generation are used for ball milling the raw material mixed powder, and after the ball milling, the grinding balls are screened out to obtain the raw material mixed powder after ball milling;

[0031] The purity of magnesium powder is 95%, the particle size is 5μm, the purity of amorphous boron powder is 95%, the par...

Embodiment 2

[0045] Step 1. According to MgB 2 MgB in wire preparation process 4 Magnesium, boron and carbon molar ratios required for powder generation Weigh magnesium powder, amorphous boron powder and nano-carbon powder into a ball mill and mix them, and then mix them according to MgB 2 MgB in wire preparation process 4 The mass ratio of raw materials and grinding balls required for powder generation is put into the grinding balls, and finally the ball mill tank containing the raw materials and grinding balls is sealed and fixed to the planetary ball mill, according to MgB 2 MgB in wire preparation process 4 The ball milling rate and ball milling time required for powder generation are used for ball milling the raw material mixed powder, and after the ball milling, the grinding balls are screened out to obtain the raw material mixed powder after ball milling;

[0046] The purity of magnesium powder is 99%, the particle size is 10μm, the purity of amorphous boron powder is 98.5%, the ...

Embodiment 3

[0060] Step 1. According to MgB 2 MgB in wire preparation process 4 Magnesium, boron and carbon molar ratios required for powder generation Weigh magnesium powder, amorphous boron powder and nano-carbon powder into a ball mill and mix them, and then mix them according to MgB 2 MgB in wire preparation process 4 The mass ratio of raw materials and grinding balls required for powder generation is put into the grinding balls, and finally the ball mill tank containing the raw materials and grinding balls is sealed and fixed to the planetary ball mill, according to MgB 2 MgB in wire preparation process 4 The ball milling rate and ball milling time required for powder generation are used for ball milling the raw material mixed powder, and after the ball milling, the grinding balls are screened out to obtain the raw material mixed powder after ball milling;

[0061] The purity of magnesium powder is 99.8%, the particle size is 20μm, the purity of amorphous boron powder is 98.5%, th...

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Abstract

Disclosed is a magnesium diffusion preparation method for a magnesium diboride superconducting wire rod based on MgB<4> precursor powder. The preparation method is based on a center magnesium diffusion technology; and MgB<4> is used as the precursor powder to replace the conventional boron precursor powder. The preparation method mainly comprises the steps of 1, performing ball milling and uniform mixing on original powder, then pressing the mixed powder into circular sheets by a powder compressing machine, and finally performing vacuum sintering and crushing on the circular sheets to obtain MgB<4> powder; and 2, fixing a magnesium rod in the center of a metal tube, filling the space between the magnesium rod and the metal tube with the MgB<4> powder, sealing the two ends of the tube, and then carrying out rotary calcining, pulling and drawing and vacuum thermal processing to obtain a MgB<2> wire rod. The MgB<2> wire rod superconducting core prepared by the preparation method is high in density; and meanwhile, the MgB<2> wire rod has high critical current density, superconducting phase filling rate and engineering critical current density, and excellent superconducting performance in medium and high magnetic fields.

Description

technical field [0001] The invention relates to a preparation method of a magnesium diboride superconducting wire. Background technique [0002] Since 2001 magnesium diboride (MgB 2 ) Since the discovery of superconductivity, this superconducting material has attracted scientists from all over the world to conduct in-depth research on it. MgB 2 Due to its simple structure, low cost, high critical transition temperature (39K), long coherence length, high upper critical field, and no weak connection at grain boundaries, superconducting materials are widely used in superconducting power, electronic devices and medical instruments. In particular, NMR imaging magnets have broad application prospects. At present, the international superconducting community has a great understanding of MgB 2 Consensus has been reached: Combined refrigeration cost and material cost, MgB 2 Superconducting materials are applied in the range of 20-25K, 1-3T magnetic field, and the advantages are v...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01B13/00H01B12/04
CPCH01B12/04H01B13/00Y02E40/60
Inventor 马衍伟徐达王栋樑张现平
Owner INST OF ELECTRICAL ENG CHINESE ACAD OF SCI
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