A device for treating carbon tetrachloride in groundwater and its working method
A technology of carbon tetrachloride and material distributing device, which is applied in chemical instruments and methods, water/sewage treatment, water/sludge/sewage treatment, etc., which can solve the problems of reduced production efficiency, low processing accuracy, and reduced system reliability and other issues, to achieve the effects of low cost and energy consumption, high processing and manufacturing precision, and avoiding manual misoperation
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Embodiment 1
[0060] Manufacture the adjustment shaft 4-4 of the present invention according to the following steps, and in parts by weight:
[0061]Step 1: Add 1950 parts of ultrapure water with a conductivity of 5.25μS / cm into the reactor, start the stirrer in the reactor at a speed of 97rpm, start the heating pump, and raise the temperature in the reactor to 114°C; add in sequence 156 parts of methyl 3-(methyl 2-(benzylcarbamoyl)acetyl)propionate, 66 parts of 4-[2,4-bis(1,1-dimethylpropyl)phenoxy]butanoic acid Parts, 76 parts of tert-butyl 4-(1-hydroxy-4-oxocyclohexyl)phenylcarbamate, stir until completely dissolved, adjust the pH value to 6.2, adjust the stirrer speed to 157rpm, and the temperature is 143°C, Esterification for 10 hours;
[0062] Step 2: Take 116 parts of 3-(N,N-dihydroxyethyl)amino-4-methoxyacetanilide, tert-butyl 5-amino-2-(dimethylamino)benzylmethylcarbamate 113 parts were pulverized, and the particle size of the powder was 830 meshes; 230 parts of N-(5-chloro-2-met...
Embodiment 2
[0067] Manufacture the adjustment shaft 4-4 of the present invention according to the following steps, and in parts by weight:
[0068] Step 1: Add 2630 parts of ultrapure water with a conductivity of 6.67μS / cm into the reactor, start the stirrer in the reactor at a speed of 146rpm, start the heating pump, and raise the temperature in the reactor to 141°C; add in sequence 187 parts of methyl 3-(methyl 2-(benzylcarbamoyl)acetyl)propionate, 123 parts of 4-[2,4-bis(1,1-dimethylpropyl)phenoxy]butanoic acid Parts, 171 parts of tert-butyl 4-(1-hydroxy-4-oxocyclohexyl)phenylcarbamate, stir until completely dissolved, adjust the pH value to 9.6, adjust the stirrer speed to 193rpm, and the temperature is 172°C, Esterification reaction for 20 hours;
[0069] Step 2: Take 211 parts of 3-(N,N-dihydroxyethyl)amino-4-methoxyacetanilide, tert-butyl 5-amino-2-(dimethylamino)benzylmethylcarbamate 198 parts were pulverized, and the particle size of the powder was 1270 mesh; 292 parts of N-(5-...
Embodiment 3
[0074] Manufacture the adjustment shaft 4-4 of the present invention according to the following steps, and in parts by weight:
[0075] Step 1: Add 2290 parts of ultrapure water with a conductivity of 5.96μS / cm into the reactor, start the stirrer in the reactor at a speed of 121rpm, start the heating pump, and raise the temperature in the reactor to 127°C; add in sequence 171 parts of methyl 3-(methyl 2-(benzylcarbamoyl)acetyl)propionate, 94 parts of 4-[2,4-bis(1,1-dimethylpropyl)phenoxy]butanoic acid Parts, 123 parts of tert-butyl 4-(1-hydroxy-4-oxocyclohexyl)phenylcarbamate, stir until completely dissolved, adjust the pH value to 7.8, adjust the stirrer speed to 175rpm, and the temperature is 157°C, Esterification for 15 hours;
[0076] Step 2: Take 163 parts of 3-(N,N-dihydroxyethyl)amino-4-methoxyacetanilide, tert-butyl 5-amino-2-(dimethylamino)benzylmethylcarbamate 155 parts were pulverized, and the particle size of the powder was 1050 mesh; 161 parts of N-(5-chloro-2-m...
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