Method for enhancing milk flavor of oil and fat and enhancing milk flavor of food and drink
A milk-flavored and food-drinking technology, which is applied in the direction of baked food, edible oil/fat, and edible oil/fat. It can solve the problems of poor physical properties of margarine, rising prices, and influence, so as to inhibit the deterioration of flavor and enhance milk. flavor effect
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[0063] Preparation method of acetonitrile soluble fraction)
[0064] 1. Add 15 ml of acetonitrile to 15 g of a sample to which δ-tridecalactone was added as an internal standard, and shake and stir thoroughly.
[0065] 2. After centrifugation at 2000 r.p.m. for 10 minutes, recover the supernatant. This operation was repeated three times, and the obtained supernatant was desolvated by a rotary evaporator (below 60° C.) under reduced pressure and blown with nitrogen to obtain acetonitrile-soluble components.
[0066] Silicone treatment method)
[0067] 1. Silica gel (InertSep SI FF 200mg / 3ml: GLSciences) was equilibrated 3 times with 2ml pentane.
[0068] 2. Add 50 μl of pentane to 50 μl of acetonitrile soluble fraction, mix well and add to silica gel.
[0069] 3. After elution with 6 ml of pentane / diethyl ether=95 / 5 and 6 ml of pentane / diethyl ether=90 / 10, then elution with pentane / diethyl ether=80 / 20.
[0070] 4. The fraction eluted with 6 ml of pentane / diethyl ether=80...
Embodiment
[0082] Examples and comparative examples of the present invention are shown below to further clarify the effects of the present invention.
[0083] (preparation of milk fat)
[0084] Four-leaf butter was heated in a water bath at 57 to 62° C., and the separated oil phase was filtered to prepare milk fat (comparative example 1). In this milk fat, the water content is 668 weight ppm, the free butyric acid content is 0.5 weight ppm, the acid value is 0.7, and the peroxide value is below the detection limit (detection limit: 0.4 meq / Kg). Refreshing natural frankincense scent. In addition, Comparative Example 1 shown in the table below is an analysis value of the milk fat to which no δ-lactones, methyl ketones, and butyric acid were added. In addition, this milk fat was also applied to the comparative example other than the Example and the comparative example 1.
[0085] (Preparation of transesterified fat A)
[0086] A blended oil of palm oil and palm kernel olein (parme olein...
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