Positive photosensitive resin composition
A technology of photosensitive resin and composition, applied in photosensitive material processing, optics, photomechanical equipment, etc., can solve problems such as low cured film characteristics, difficulty in chemical resistance and adhesiveness, and inability to cope with the production of packaging , to achieve the effect of excellent liquid resistance
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[0211] Hereinafter, based on an Example and a comparative example, this invention is demonstrated further concretely. It should be noted that the present invention is not limited to the following examples.
Synthetic example 1
[0213] [(a) Ingredient: polybenzo Synthesis of azole precursor (polymer I)]
[0214] Into a 0.2-liter flask equipped with a stirrer and a thermometer, 60 g of N-methylpyrrolidone was charged, 13.92 g (38 mmol) of 2,2-bis(3-amino-4-hydroxyphenyl)hexafluoropropane was added, and stirred to dissolve. Next, while maintaining the temperature at 0 to 5°C, 7.48 g (28 mmol) of dodecane dichloride and 3.56 g (12 mmol) of 4,4'-diphenyl ether dichloride were added dropwise over 10 minutes. , and the solution in the flask was stirred for 60 minutes. The above solution was dropped into 3 liters of water, the precipitate was recovered, washed 3 times with pure water, and then decompressed to obtain a polybenzoic acid having a structure represented by formula (1). An azole precursor (hereinafter referred to as polymer I). The weight-average molecular weight of the polymer I was calculated in terms of standard polystyrene using gel permeation chromatography (GPC), and it was 42,000, and ...
Synthetic example 2
[0228] [(a) Ingredient: polybenzo Synthesis of azole precursor (polymer II)]
[0229] In addition to replacing 7.48 g (28 mmol) of dodecanoyl dichloride and 3.56 g (12 mmol) of 4,4'-diphenyl ether dichloride used in Synthesis Example 1 with sebacoyl chloride (40 mmol), and Synthesis example 1 is synthesized similarly, obtains the polybenzoic acid having the structure represented by formula (1) An azole precursor (hereinafter referred to as polymer II). Polymer II had a weight average molecular weight of 38,000 and a dispersity of 2.0.
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