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A kind of preparation method of acrylamide-bentonite capsule loaded with corrosion inhibitor

A technology of acrylamide and corrosion inhibitor, which is applied in the field of preparation of acrylamide-bentonite capsules, can solve problems such as damaging equipment, affecting production, and economic loss, and achieves the effect of increasing strength

Active Publication Date: 2021-06-25
SOUTHWEAT UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, carbon dioxide dissolved in formation water will generate an acidic solution, and the oil well environment is characterized by acidity, high temperature, high pressure, and high salinity, resulting in high corrosion rate general corrosion and severe localized perforation corrosion of oil well pipelines
In the process of oil and gas exploitation, corrosion is a very prominent problem. Corrosion not only damages equipment, increases maintenance and operating costs, affects production, pollutes products, etc., but also often causes major accidents and causes huge economic losses.

Method used

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  • A kind of preparation method of acrylamide-bentonite capsule loaded with corrosion inhibitor
  • A kind of preparation method of acrylamide-bentonite capsule loaded with corrosion inhibitor
  • A kind of preparation method of acrylamide-bentonite capsule loaded with corrosion inhibitor

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] A preparation method of an acrylamide-bentonite capsule loaded with a corrosion inhibitor, comprising the following steps:

[0031] Step 1. In parts by weight, take 8 parts of chitosan powder and place it in an oven for drying, sieve to remove impurities, then add 50 parts of deionized water and 2 parts of liquid corrosion inhibitor, and continuously stir at 80°C for 50 minutes. Obtain the mixture solution, dry and concentrate the mixture solution to 35% of the original volume in an oven to obtain a viscous mixture, inject the viscous mixture into a spherical container through a syringe, dry and solidify into a spherical shape, and obtain the corrosion inhibitor; the chitosan The molecular weight of the powder is 100,000; the liquid corrosion inhibitor is corrosion inhibitor FJH-08;

[0032] Step 2. Prepare an aqueous solution of acrylamide. In parts by weight, add 0.3 parts of a crosslinking agent, 0.005 parts of an initiator and 15 parts of bentonite to 50 parts of an...

Embodiment 2

[0034] A preparation method of an acrylamide-bentonite capsule loaded with a corrosion inhibitor, comprising the following steps:

[0035] Step 1. In parts by weight, take 10 parts of chitosan powder and place it in an oven for drying, sieve to remove impurities, then add 60 parts of deionized water and 3 parts of liquid corrosion inhibitor, and continuously stir at 75°C for 60 minutes. Obtain the mixture solution, dry and concentrate the mixture solution to 40% of the original volume in an oven to obtain a viscous mixture, inject the viscous mixture into a spherical container through a syringe, dry and solidify into a spherical shape, and obtain the corrosion inhibitor; the chitosan The molecular weight of the powder is 100,000; the liquid corrosion inhibitor is corrosion inhibitor FJH-08;

[0036] Step 2. Prepare an aqueous solution of acrylamide. Add 0.4 parts of a crosslinking agent, 0.006 parts of an initiator and 12 parts of bentonite to 60 parts of an aqueous solution o...

Embodiment 3

[0038] A preparation method of an acrylamide-bentonite capsule loaded with a corrosion inhibitor, comprising the following steps:

[0039]Step 1. In parts by weight, take 8 parts of chitosan powder and place it in an oven for drying, sieve to remove impurities, then add 50 parts of deionized water and 2 parts of liquid corrosion inhibitor, and continuously stir at 80°C for 50 minutes. Obtain the mixture solution, dry and concentrate the mixture solution to 35% of the original volume in an oven to obtain a viscous mixture, inject the viscous mixture into a spherical container through a syringe, dry and solidify into a spherical shape, and obtain the corrosion inhibitor; put the corrosion inhibitor in Processed in a low-temperature plasma processor for 30 minutes, the atmosphere of the low-temperature plasma processor was argon; the frequency of the low-temperature plasma processor was 40KHz, the power was 50W, and the pressure of argon was 45Pa; the shell poly The molecular wei...

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Abstract

The invention discloses a preparation method of an acrylamide-bentonite capsule loaded with a corrosion inhibitor, comprising: taking chitosan powder, placing it in an oven for drying, sieving to remove impurities, and then adding deionized water and a liquid corrosion inhibitor , Stir continuously at 65-85°C to obtain a mixture solution, dry and concentrate the mixture solution in an oven to 30-40% of the original volume to obtain a viscous mixture, inject the viscous mixture into a spherical container through a syringe, dry and solidify into a spherical shape , to obtain the corrosion inhibitor; prepare an aqueous solution of acrylamide, add crosslinking agent, initiator and bentonite to the aqueous solution of acrylamide, mix evenly, and apply the obtained mixed solution on the surface of the cured corrosion inhibitor, and carry out the process under vacuum and high temperature. Cross-linking reaction, the reaction product is dried, and the capsule loaded with corrosion inhibitor acrylamide-bentonite is obtained; the bentonite of the present invention is used as the capsule skeleton, thereby greatly increasing the strength of the capsule, and can be more stable and firm under high temperature and high pressure downhole .

Description

technical field [0001] The invention belongs to the field of composite material preparation, and in particular relates to a preparation method of an acrylamide-bentonite capsule loaded with a corrosion inhibitor. Background technique [0002] In the petroleum industry, carbon dioxide is usually injected into oil storage formations to enhance oil recovery. Firstly, the injection of carbon dioxide into the oil layer can maintain the formation pressure and displace crude oil to the production well; secondly, the CO 2 It has many advantages such as low viscosity, strong extraction ability and strong injection ability. CO 2 It can have physical and chemical interactions with underground fluids, resulting in the expansion of crude oil volume, the decrease of viscosity and the increase of water viscosity. Under certain conditions, carbon dioxide can be miscible with crude oil, greatly reducing interfacial tension, thereby enhancing oil recovery. However, carbon dioxide dissolve...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K8/54C08F220/56C08F222/38
CPCY02P20/54
Inventor 张红平崔国栋杨波张亚萍唐苹苹刘彬瑶
Owner SOUTHWEAT UNIV OF SCI & TECH