A kind of botanical compound rice stem borer insecticide and preparation method thereof
A technology of insecticide and stem borer, which is applied in the field of plant source compounded stem borer insecticide and its preparation, can solve problems such as environmental pollution and excessive pesticide residues, and achieve simple and effective preparation methods, small environmental hazards, The effect of a wide range of material sources
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Embodiment 1
[0014] The preparation of compound insecticide of the present invention:
[0015] (1) Dried S. chinensis and Licewort respectively in an oven at 55°C to constant weight, then pulverized, passed through a 60-mesh sieve, and set aside;
[0016] (2) Take 50g of the sieve prepared in step (1) and add 10 times the amount of 75% ethanol, then place them in a conical flask for extraction for 48 hours, and then use ultrasonic waves (power 300W, frequency 40kHZ, temperature 40°C) to extract for 30 minutes, The filter residue was repeated three times, and suction filtered to obtain the S. chinensis filtrate and Licetium filtrate, which were set aside;
[0017] (3) Place the filtrate obtained in step (2) on a rotary evaporator to control the temperature at 55°C for distillation under reduced pressure. When no solvent flows out, collect the extract, and dry the extract in an oven at 60°C until constant Heavy, to obtain the extract of Snakevine and Licewort extract for use;
[0018] (4) ...
Embodiment 2
[0024] The preparation of the single compound insecticide of the extract of S. chinensis:
[0025] (1) Collect 1 g of the extract of S. chinensis in Example 1, add 1 g of co-solvent, 98 mL of distilled water, seal it and let it stand at room temperature for 1 hour, and then treat it with ultrasonic waves (power 300W, frequency 59kHZ, temperature 45°C) for 20 minutes;
[0026] (2) After stirring for 15 minutes, the single compound insecticide stock solution of the extract of S. chinensis can be obtained, and the concentration is 10g / L;
[0027] (3) After pre-experiment and under the conditions of saving raw materials and good insecticidal effect, after the stock solution of the single insecticide of S. chinensis extract was diluted 5.3 times, the optimum concentration of 1.88g / L of S. Determination of insect activity can obtain the single compound insecticide of the extract of S. chinensis.
Embodiment 3
[0029] Preparation of lice grass extract single compound insecticide:
[0030] (1)(2) is the same as (1)(2) in embodiment two;
[0031] (3) After pre-experiment and under the conditions of saving raw materials and good insecticidal effect, after diluting 6.6 times of single insecticide stock solution of licewort extract, choose the optimal concentration of 1.52g / L for indoor insecticide. After the activity measurement, the single compound insecticide of the lice grass extract can be obtained.
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