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35results about How to "High sensitivity response" patented technology

Preparation method of graphite oxide phase carbon nitride modified electrode and application of electrode in detection of heavy metal ions

The invention relates to a preparation method of a graphite oxide phase carbon nitride modified electrode. The preparation method comprises the following steps: (1) preparing graphite oxide phase carbon nitride; and (2) preparing a graphite oxide phase carbon nitride sensor. The electrode is applied to detecting heavy metal ions. Graphite oxide phase carbon is of a three-dimensional hole structure which is large in specific surface area and contains hydrophilic groups such as hydroxyl, carboxyl, and epoxy groups. The graphite oxide phase carbon is applied to an electrochemical sensor. The heavy metal ions Cu<2+> are detected by virtue of a different pulse stripping voltammetry, and influence of factors such as enriching time, enriching potential, the pH value of a solution, and modification amount on stripping peak current can be optimized. Under an experimental condition that the enriching time is 300s, the enriching potential is -0.6V, the pH value of the solution is 4.68 and the modification amount is 12 microliters, a standard curve represents a good linear relationship, wherein the linear range is (1.60*10<-15>-6.31*10<-15>mol/L, the linear equation is ip(microA)=1.2533C(micro mol/L)+6.2232, the correlation coefficient (R) is 0.9989, and the limit of detection (S/N=3) reaches 1*10<-16>mol/l. The electrode has ultrahigh sensitivity to heavy metal ion detection.
Owner:YANGZHOU UNIV

Method for preparing hydrogen sensitive element based on quadrature-phase molybdenum oxide nano-belt

The invention provides a method for preparing a hydrogen sensitive element based on a quadrature-phase molybdenum oxide nano-belt. The method comprises the following steps: A, a quadrature-phase molybdenum oxide nano-belt powder by a hydrothermal method; B, preparing an interdigital electrode by a photolithographic mask method; and C assembling a hydrogen sensitive element, namely molybdenum oxide powder and an absolute ethyl alcohol mixed liquid, carrying out ultrasonic treatment, dropwise adding the mixed liquid into the center position of the interdigital electrode, and annealing. According to the method, Na2MoO4.2H20 is used as a raw material, the quadrature-phase molybdenum oxide nano-belt with uniform appearance is prepared by adopting the simple hydrothermal method, the using process is simple, the preparation cycle is short, the sample yield is high, and the cost is low; the nano-belt dispersed by ultrasonics is coated to the interdigital electrode to obtain the hydrogen sensitive element with excellent performance; at room temperature, the element has the characteristics of high sensitivity and quick response on low-concentration hydrogen, has excellent repeatability and selectivity on hydrogen, and can meet the requirement of quickly detecting low-concentration hydrogen.
Owner:HUBEI UNIV

Preparation method of alpha-oxoglutarate fluorescent/ultraviolet molecular probe and application of alpha-oxoglutarate fluorescent/ultraviolet molecular probe to biological samples

The invention relates to a preparation method of an alpha-oxoglutarate fluorescent / ultraviolet molecular probe and application of the alpha-oxoglutarate fluorescent / ultraviolet molecular probe to biological samples. The preparation method includes the steps that NBD-Cl is dissolved in chloroform, the dissolution concentration is 0002-0.012 g / ml, then a hydrazine hydrate-methanol solution with the volume concentration being 0.2-1.2% is added in and uniformly mixed, brown precipitate is obtained through stirring at room temperature and filtered, a filter cake is washed through ethyl acetate and dried, and the brown product alpha-oxoglutarate fluorescent / ultraviolet molecular probe is obtained. The alpha-oxoglutarate fluorescent / ultraviolet molecular probe is applicable to qualitatively and quantitatively analyzing alpha-oxoglutarate in the biological samples, and detection is sensitive, accurate and fast. The biological samples mainly comprise serum, living cells, muscle tissue and the like. The alpha-oxoglutarate fluorescent / ultraviolet molecular probe can be applied to analytical chemistry, life organic analysis, disease pre-diagnosis, medical clinical inspection and other related fields. The alpha-oxoglutarate fluorescent / ultraviolet molecular probe has the advantages of being good in response performance and high in data accuracy, repeatability and precision, equipment is convenient, fast and easy to operate, operability is high, and the alpha-oxoglutarate fluorescent / ultraviolet molecular probe is particularly suitable for large-batch sample combined screening and other large-data research.
Owner:QUFU NORMAL UNIV

Temperature-sensitive-type terahertz detector based on phase change material and preparation method

The invention discloses a temperature-sensitive-type terahertz detector based on phase change material and a preparation method. The detector is composed of an alumina substrate, an indium antimonide-sensitive element, a vanadium dioxide grating structure layer, a half-wave antenna and a device socket. According to the temperature-sensitive-type terahertz detector prepared according to the invention, the vanadium dioxide grating structure layer is introduced on the basis of a traditional metal-semiconductor-metal structure, the phase change transition characteristic of vanadium dioxide at an ambient temperature of 68 DEG C is used, thus a drastic change of conductivity of the grating structure layer is caused, then field enhancement effects caused by local plasmons of the whole device areenabled to be different, and a modulation purpose of terahertz wave detection is achieved; and a new function of sensing the ambient temperature is added while fast highly-sensitive response of a widewave band of 0.01- 3THZ is realized. The detector has very important significance for both device structure design optimization and device function perfection, and can play important roles in the fields of science, technology and the like.
Owner:SHANGHAI INST OF TECHNICAL PHYSICS - CHINESE ACAD OF SCI

Supporting column-supported echo wall mode photonics device, preparation method thereof and use of device

The invention belongs to the photonics device field and relates to a supporting column-supported echo wall mode photonics device, a preparation method thereof and the use of the device. In particular,the present invention provides a supporting column-supported micro disk. The supporting column of the supporting column-supported micro disk comprises a first electron beam resist; the micro disk comprises a second electron beam resist; and the molecular weight of the first electron beam resist is lower than that of the second electron beam resist. The supporting column-supported micro disk, a micro disk array structure, an echo wall mode optical resonant micro-cavity and a photonics device of the invention have the advantages of simple preparation process, convenient operation and low cost,and can be prepared on a large scale, have high quality factors and spectral modulation functions. With the preparation method adopted, a problem that a substrate needs to be separately etched in a traditional high-quality micro-cavity preparation process can be solved; and the coupling effect of a plurality of micro-cavities can be realized. The method has high practicability, and is especially suitable for the design and application of photonics integrated components.
Owner:INST OF CHEM CHINESE ACAD OF SCI

Zinc tungstate/zinc oxide heterogeneous nanofiber as well as preparation method and application thereof

The invention discloses zinc tungstate/zinc oxide heterogeneous nanofiber as well as a preparation method and application thereof. The preparation method comprises the steps that the molar weight of zinc nitrate is fixed in an electrostatic spinning precursor solution, the molar weight of phosphotungstic acid is regulated and controlled, the precursor solution is mixed and stirred to be uniform, then electrostatic spinning is conducted, and calcination is conducted in air, so that the zinc tungstate/zinc oxide heterogeneous nanofiber synthesized with the assistance of polyoxometallate is obtained. The one-dimensional heterogeneous nanofiber is composed of zinc tungstate and zinc oxide compounded with the zinc tungstate, and has an n-n type heterogeneous nanofiber structure. When the heterogeneous nanofiber is used as a gas sensitive sensor, a gas sensitive test result shows that the gas sensitive sensor has the characteristic of high-sensitivity quick response to triethylamine. In combination with excellent electron transfer performance and large specific surface area of the zinc tungstate/zinc oxide heterogeneous nanofiber, the gas sensitive sensor can realize high-selectivity, high-sensitivity and long-term stable detection of the triethylamine.
Owner:ANHUI UNIVERSITY

Preparation method of fluorescent/ultraviolet molecular probe for alpha-ketoglutarate and its application in biological samples

The invention relates to a preparation method of an alpha-oxoglutarate fluorescent / ultraviolet molecular probe and application of the alpha-oxoglutarate fluorescent / ultraviolet molecular probe to biological samples. The preparation method includes the steps that NBD-Cl is dissolved in chloroform, the dissolution concentration is 0002-0.012 g / ml, then a hydrazine hydrate-methanol solution with the volume concentration being 0.2-1.2% is added in and uniformly mixed, brown precipitate is obtained through stirring at room temperature and filtered, a filter cake is washed through ethyl acetate and dried, and the brown product alpha-oxoglutarate fluorescent / ultraviolet molecular probe is obtained. The alpha-oxoglutarate fluorescent / ultraviolet molecular probe is applicable to qualitatively and quantitatively analyzing alpha-oxoglutarate in the biological samples, and detection is sensitive, accurate and fast. The biological samples mainly comprise serum, living cells, muscle tissue and the like. The alpha-oxoglutarate fluorescent / ultraviolet molecular probe can be applied to analytical chemistry, life organic analysis, disease pre-diagnosis, medical clinical inspection and other related fields. The alpha-oxoglutarate fluorescent / ultraviolet molecular probe has the advantages of being good in response performance and high in data accuracy, repeatability and precision, equipment is convenient, fast and easy to operate, operability is high, and the alpha-oxoglutarate fluorescent / ultraviolet molecular probe is particularly suitable for large-batch sample combined screening and other large-data research.
Owner:QUFU NORMAL UNIV

Zigbee-based wireless slip ring device and nucleic acid detection method thereof

The invention provides a zigbee-based wireless slip ring device and a nucleic acid detection method thereof. The zigbee-based wireless slip ring device comprises a dynamic sending platform, a power driving mechanism and a static receiving platform, a longitudinal and transverse servo motor and a system receiving plate are arranged on the static receiving platform, and the bottom of the static receiving platform is connected with a driving lifting assembly and a driven telescopic arm; and a triangular supporting frame is arranged at the bottom of the active lifting assembly, the dynamic sending platform is connected to the lower portion of the triangular supporting frame and provided with a lithium battery and a system sending plate, and a fluorescent quantitative PCR amplification instrument is installed on the bottom face of the dynamic platform and comprises exposed probes, a built-in fluorescent lamp, a photoelectric conversion module and a thermoelectric cooler. The zigbee-based wireless slip ring device has the beneficial effects that in the process of transmitting digital and analog signals of the dynamic platform to the static platform, a motor drives master and slave arms and linkages a holding and clamping device to keep the telescopic range, the problems that wiring cannot be conducted on an automatic intelligent slip ring device for the cold-chain food and signals at certain distances are interconnected are solved, and the effects that when the signals are not delayed, the data transmission is fast is achieved.
Owner:ZHONGBEI UNIV +1

Receiving transducer with adjustable working frequency

The invention discloses a receiving transducer with adjustable working frequency which comprises a plurality of coupled Helmholtz resonant cavity structure units which are arranged together. Each coupling Helmholtz resonant cavity structure unit comprises a thin-wall circular tube extension neck, a piezoelectric material and two coupled Helmholtz resonant cavities. Each Helmholtz resonant cavity comprises a perforated top wall, a non-perforated bottom wall, a side wall, a front panel and a rear panel. Each side wall is located between the two coupled Helmholtz resonant cavity structure units,and each front panel and each rear panel are used for forming a closed cavity; openings in the top walls of the two Helmholtz resonant cavities are the same or different in size, thin-wall circular tube extension necks are arranged in the openings in the top walls in a penetrating mode, piezoelectric materials are arranged between the two Helmholtz resonant cavities, and the piezoelectric materials are formed by pressing piezoelectric ceramic pieces and electrode pieces. The whole structure and the manufacturing process are simple, array processing is easy to achieve to improve the sensitivity, series-parallel connection processing can be conducted according to needs, and the cost is low.
Owner:SHAANXI NORMAL UNIV

A receiving transducer with adjustable working frequency

The invention discloses a receiving transducer with adjustable working frequency, which comprises a plurality of coupled Helmholtz resonant cavity structural units arranged together, and the coupled Helmholtz resonant cavity structural unit includes a thin-walled circular tube extension neck, A piezoelectric material and two coupled Helmholtz resonant cavities, the Helmholtz resonant cavity includes a top wall with openings, a bottom wall without openings, side walls, and a front panel and a rear panel, the The side wall is located between the two coupled Helmholtz resonant cavity structural units, and the front panel and the rear panel are used to form a closed cavity; the openings of the top walls of the two Helmholtz resonant cavities have the same or different sizes, In addition, an extension neck of a thin-walled circular tube is interspersed in the opening of the top wall, and a piezoelectric material is arranged between the two Helmholtz resonant cavities, and the piezoelectric material is formed by pressing piezoelectric ceramic sheets and electrode sheets. The overall structure and manufacturing process of the present invention are simple, easy to be processed in an array to improve sensitivity, and can also be processed in series and parallel according to needs, and the cost is low.
Owner:SHAANXI NORMAL UNIV

A kind of whispering gallery mode photonics device supported by pillars and its preparation method and application

The invention belongs to the photonics device field and relates to a supporting column-supported echo wall mode photonics device, a preparation method thereof and the use of the device. In particular,the present invention provides a supporting column-supported micro disk. The supporting column of the supporting column-supported micro disk comprises a first electron beam resist; the micro disk comprises a second electron beam resist; and the molecular weight of the first electron beam resist is lower than that of the second electron beam resist. The supporting column-supported micro disk, a micro disk array structure, an echo wall mode optical resonant micro-cavity and a photonics device of the invention have the advantages of simple preparation process, convenient operation and low cost,and can be prepared on a large scale, have high quality factors and spectral modulation functions. With the preparation method adopted, a problem that a substrate needs to be separately etched in a traditional high-quality micro-cavity preparation process can be solved; and the coupling effect of a plurality of micro-cavities can be realized. The method has high practicability, and is especially suitable for the design and application of photonics integrated components.
Owner:INST OF CHEM CHINESE ACAD OF SCI

A preparation method of hydrogen sensitive element based on orthorhombic phase molybdenum oxide nanoribbon

The invention provides a method for preparing a hydrogen sensitive element based on a quadrature-phase molybdenum oxide nano-belt. The method comprises the following steps: A, a quadrature-phase molybdenum oxide nano-belt powder by a hydrothermal method; B, preparing an interdigital electrode by a photolithographic mask method; and C assembling a hydrogen sensitive element, namely molybdenum oxide powder and an absolute ethyl alcohol mixed liquid, carrying out ultrasonic treatment, dropwise adding the mixed liquid into the center position of the interdigital electrode, and annealing. According to the method, Na2MoO4.2H20 is used as a raw material, the quadrature-phase molybdenum oxide nano-belt with uniform appearance is prepared by adopting the simple hydrothermal method, the using process is simple, the preparation cycle is short, the sample yield is high, and the cost is low; the nano-belt dispersed by ultrasonics is coated to the interdigital electrode to obtain the hydrogen sensitive element with excellent performance; at room temperature, the element has the characteristics of high sensitivity and quick response on low-concentration hydrogen, has excellent repeatability and selectivity on hydrogen, and can meet the requirement of quickly detecting low-concentration hydrogen.
Owner:HUBEI UNIV
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