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Multifunctional organic silicon finishing agent and preparation method thereof

A technology of organosilicon and finishing agent, which is applied in fiber treatment, textiles and papermaking, etc., to achieve the effects of cost reduction, excellent anti-ultraviolet performance and good whiteness

Inactive Publication Date: 2012-09-26
NANTONG UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, there are relatively few developments on the comprehensive functions of silicone finishing agents such as anti-ultraviolet, anti-yellowing, soft and smooth.

Method used

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  • Multifunctional organic silicon finishing agent and preparation method thereof
  • Multifunctional organic silicon finishing agent and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] A multifunctional silicone finishing agent, which comprises the following components in mass percent: 20% of anti-ultraviolet polyether silicone oil, 8% of isobutanol, phosphate betaine type gemini surfactant and fatty alcohol polyoxyethylene ether (10 ) 1:1 compound emulsifier 8%, pH buffer 5%, deionized water 59%.

[0018] The preparation method of the above-mentioned multifunctional organosilicon finishing agent comprises the following steps:

[0019] 1. Take 100 parts of water-soluble silicone containing epoxy groups, add 100 parts of light-stabilizing substances-N-butyl-tetramethylpiperidinamine or tetramethylpiperidinol compounds, and heat up to 70 After reacting for 4 hours at ℃, raise the temperature to 120℃, react for 6 hours, and discharge the material to obtain a colorless to slightly yellow transparent finished product, which is the anti-ultraviolet polyether modified silicone oil;

[0020] 2. Add metered deionized water, phosphate betaine type gemini surfa...

Embodiment 2

[0022] A multifunctional silicone finishing agent, which comprises the following components in mass percent: 14% of anti-ultraviolet polyether silicone oil, 10% of isobutanol, phosphate betaine type gemini surfactant and fatty alcohol polyoxyethylene ether (10 ) 1:1 compound emulsifier 9%, pH value buffer 3.5%, deionized water 63.5%.

[0023] The preparation method of the above-mentioned multifunctional organosilicon finishing agent comprises the following steps:

[0024] 1. Take 100 parts of water-soluble silicone containing epoxy groups, add 200 parts of N-butyl-tetramethylpiperidinamine or tetramethylpiperidinol compounds with light stabilizing effect, and heat up to 80°C After reacting for 4.5 hours, raise the temperature to 125°C, react for 7 hours, and discharge the material to obtain a colorless to slightly yellow transparent finished product, which is the anti-ultraviolet polyether modified silicone oil;

[0025] 2. Add metered deionized water, phosphate betaine type ...

Embodiment 3

[0027] A multifunctional silicone finishing agent, which comprises the following components in mass percentage: 8% of anti-ultraviolet polyether silicone oil, 12% of isobutanol, phosphate betaine type gemini surfactant and fatty alcohol polyoxyethylene ether (10 ) 1:1 compound emulsifier 10%, pH value buffer 2%, deionized water 68%.

[0028] The preparation method of the above-mentioned multifunctional organosilicon finishing agent comprises the following steps:

[0029] 1. Take 100 parts of water-soluble silicone containing epoxy groups, add 300 parts of light-stabilizing substances-N-butyl-tetramethylpiperidinamine or tetramethylpiperidinol compounds, and heat up to 90 After reacting for 5 hours at ℃, raise the temperature to 130℃, react for 8 hours, and discharge the material to obtain a colorless to slightly yellow transparent finished product, which is the anti-ultraviolet polyether modified silicone oil;

[0030] 2. Add metered deionized water and phosphate betaine type...

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Abstract

The invention discloses a multifunctional organic silicon finishing agent and a preparation method thereof. The multifunctional organic silicon finishing agent comprises the following components in percentage by mass: anti-ultraviolet polyether organic silicon oil, isobutyl alcohol, composite emulsifier of phosphate betaine type gemini surfactant and fatty alcohol-polyoxyethylene ether in a ratio of 1:1, PH buffering agent and deionized water. The preparation method for the multifunctional organic silicon finishing agent comprises the following steps of: modifying organic silicon by adopting a special heterocyclic hindered ammonia compound, substituting the conventional amino, introducing a polyether functional unit on the main chain of the organic silicon, introducing the hindered ammonia compound on the branched chain, and synthesizing multifunctional organic silicon oil. The finishing agent keeps the original advantages of the amino silicon oil, and is particularly suitable for soft finishing and anti-ultraviolet finishing of bleached fabrics and light color fabrics; and the finishing agent can be prepared into silicon oil micro-emulsion of various proper concentrations by full emulsifying and has strong usability.

Description

technical field [0001] The invention relates to a multifunctional organosilicon finishing agent and a preparation method thereof. Background technique [0002] Silicone emulsion is an important finishing agent in the process of fabric treatment. It can significantly improve the hand feel of fabrics, making them smooth and soft. In recent years, there are more fabric softening and smoothing agents based on amino silicone oil on the market. At present, there are relatively few developments on the comprehensive functions of silicone finishing agents such as anti-ultraviolet, anti-yellowing, soft and smooth. Contents of the invention [0003] Purpose of the invention: In order to solve the deficiencies of the prior art, the present invention provides a multifunctional silicone finishing agent with anti-ultraviolet and anti-yellowing functions. [0004] Another object of the present invention is to provide a method for preparing the above-mentioned multifunctional silicone fi...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06M13/513D06M13/44D06M13/17
Inventor 朱国华管永华华平李建华施磊
Owner NANTONG UNIVERSITY
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