Natural antimicrobial contained viscose fiber and preparation method thereof
A viscose fiber and antibacterial agent technology is applied in the field of antibacterial functional viscose fiber products and its preparation, and achieves the effects of large economic and social benefits, durable antibacterial function and reasonable process
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Embodiment 1
[0031] Take a certain amount of honeysuckle extract powder and add it into water at a temperature of 20° C. to dissolve at a ratio of 100 g / 1000 ml to prepare a honeysuckle extract powder solution.
[0032] The obtained honeysuckle extract powder solution is added in the viscose spinning stock solution (fiber mass fraction is 5%) with the ratio of 10% of the mass of the viscose spinning stock solution, after stirring and dispersing, leave it to stand vacuum for degassing, and then wet it as usual. Spinning and spinning process, enter 30 ℃ coagulation bath through candle filter and spinneret after measuring by metering pump, described coagulation bath is made up of 90g / L sulfuric acid, 260g / L sodium sulfate and 30g / L zinc sulfate, The total drawing ratio is 150%, the spinning speed is 50m / min, and the finished fiber is obtained after being oiled and dried, and the viscose fiber with honeysuckle antibacterial function is obtained.
Embodiment 2
[0034] Take a certain amount of honeysuckle extract powder and add it into water at a temperature of 40° C. to dissolve at a ratio of 200 g / 1000 ml to prepare a honeysuckle extract powder solution.
[0035] The obtained honeysuckle extract powder solution is added to the viscose spinning stock solution (fiber mass fraction is 10%) in the ratio of 15% of the mass of the viscose spinning stock solution, after stirring and dispersing, leave it to stand vacuum for degassing, and then according to the embodiment 1 The similar wet spinning and spinning process is formed to obtain the viscose fiber with the antibacterial function of honeysuckle.
Embodiment 3
[0037] Take a certain amount of honeysuckle extract powder and add it into water at a temperature of 60° C. to dissolve at a ratio of 300 g / 1000 ml to prepare a honeysuckle extract powder solution.
[0038] The obtained honeysuckle extract powder solution is added to the viscose spinning stock solution (fiber mass fraction is 15%) in the ratio of 20% of the mass of the viscose spinning stock solution, after stirring and dispersing, leave it to stand vacuum for degassing, and then according to the embodiment 1 The similar wet spinning and spinning process is formed to obtain the viscose fiber with the antibacterial function of honeysuckle.
[0039] Filament spinning process: the conventional wet spinning and spinning process adopted in the above-mentioned embodiments 1-3 includes the following steps: stock solution feeding and antibacterial agent blending - spinneret spinning - coagulation bath - godet roll - hot water washing - Pickling-water washing-boiling water stretching-w...
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