Atmospheric pressure easy dyeing regenerated polyester filament and its preparation method
A technology of polyester filament and normal pressure, which is applied in the field of normal pressure and easy-dyeing regenerated polyester filament and its preparation, which can solve the problems of changes in the purity, structure and performance of renewable resources, difficulty in preparing high-quality fiber products, and difficulty in continuous chemical industrial production. , to achieve the effects of promoting development and utilization, good market prospects, and reducing economic losses
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Embodiment 1
[0041] in such as figure 1 Put 10kg of polyester bottle flakes, 3kg of ethylene glycol, and n-butyl titanate accounting for 3‰ of polyester waste into the depolymerization kettle 1 shown in the reaction flow chart, and keep the temperature and pressure at 250°C under a pressure of 3kg. Carry out depolymerization reaction in 3 hours;
[0042] After the depolymerization is completed, 5% of the depolymerization product is divided into the low-temperature reactor 3, and 5% of nano-MMT and 5% of polyethylene oxide are added to react at 200° C. for 1 hour, and the reaction is completed and passed into the polymerization reactor 2;
[0043] In the polymerization kettle 2, the depolymerization product in the depolymerization kettle 1 was introduced, and at the same time, 1% of adipic acid, 7% of isophthalic acid and 200ppm of stabilizer trimethyl phosphate were added, and 5% of low temperature The product in the reaction kettle 3, raise the temperature to 235°C and vacuumize for pre-...
Embodiment 2
[0045] in such as figure 1 Put 10kg of polyester bottle flakes, 5kg of ethylene glycol, and ethylene-based alumina accounting for 5‰ of polyester waste into the depolymerization kettle 1 shown in the reaction flow chart, and keep warm and pressurized at 260°C under a pressure of 2kg. Carry out depolymerization reaction in 2 hours;
[0046] After depolymerization, divide 10% of the depolymerization product into the low-temperature reactor 3 and add 1% nano-MMT to react at 150° C. for 12 hours, and pass it into the polymerization kettle 2 after the reaction is completed;
[0047] The depolymerization product in the depolymerization kettle 1 is passed into the polymerization kettle 2, and 3% of adipic acid, 4% of isophthalic acid and 50 ppm of stabilizer triphenyl phosphite are added simultaneously, and another 20% of For the product in the low-temperature reactor 3, raise the temperature to 260°C and vacuumize for pre-condensation for 30 minutes. When the vacuum degree reaches be...
Embodiment 3
[0049] in such as figure 1 10kg of polyester bottle flakes, 5kg of ethylene glycol, and ethylene glycol antimony accounting for 5‰ of polyester waste are put into the depolymerization kettle 1 as shown in the reaction flow chart. Hours for depolymerization reaction;
[0050] After depolymerization, divide 10% of the depolymerization product into the low-temperature reactor 3 and add 1% nano-MMT to react at 150° C. for 12 hours, and pass it into the polymerization kettle 2 after the reaction is completed;
[0051] The depolymerization product in the depolymerization kettle 1 is passed into the polymerization kettle 2, and 3% of adipic acid, 4% of isophthalic acid and 50 ppm of stabilizer trimethyl phosphate are added at the same time, and 20% of low temperature The product in the reaction kettle 3, raise the temperature to 260°C and vacuumize for pre-condensation, the time is 30min, when the vacuum reaches below 100Pa, raise the temperature to 280°C for polycondensation; Spin...
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Abstract
Description
Claims
Application Information
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