A kind of preparation method of chitosan modified starch type sizing agent
A starch-type sizing agent and chitosan modification technology are applied in the preparation of chitosan-modified starch-type sizing agents and the field of preparation of sizing agents. The colorant has problems such as irritation to human skin and complex preparation process, and achieves the effects of superior chemical and thermal stability, effective diffusion and spreading, and easy access to raw materials
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Embodiment 1
[0024] A kind of preparation method of chitosan modified starch type sizing agent, the steps are as follows:
[0025] a. Put 9 parts by mass of raw starch into a reaction container, add 300 parts by mass of water, stir, heat up to 90° C., and perform a gelatinization reaction for 1 hour to obtain a starch paste;
[0026] b, get 1 mass part of chitosan and join in the starch paste, and slowly add 0.2 mass part of crosslinking agent, 0.2 mass part of plasticizer, 0.2 mass part of polyvinyl alcohol, 0.2 mass part of Sodium sulfate, the Tween 60 of 0.1 mass part, obtains mixed material;
[0027] c. React the mixed material at 90° C. for 1 hour, cool to room temperature, let it stand for 2 hours, and defoam to obtain a chitosan-modified starch-type sizing agent.
Embodiment 2
[0029] A kind of preparation method of chitosan modified starch type sizing agent, the steps are as follows:
[0030] a. Put 12 parts by mass of raw starch into a reaction container, add 300 parts by mass of water, stir, heat up to 90° C., and perform a gelatinization reaction for 1 hour to obtain a starch paste;
[0031] b, get 1 mass part of chitosan and join in the starch paste, and slowly add 0.2 mass part of crosslinking agent, 0.2 mass part of plasticizer, 0.2 mass part of polyvinyl alcohol, 0.2 mass part of Sodium sulfate, the Tween 60 of 0.1 mass part, obtains mixed material;
[0032] c. React the mixed material at 90° C. for 1 hour, cool to room temperature, let it stand for 2 hours, and defoam to obtain a chitosan-modified starch-type sizing agent.
Embodiment 3
[0034] A kind of preparation method of chitosan modified starch type sizing agent, the steps are as follows:
[0035] a. Put 15 parts by mass of raw starch into a reaction container, add 300 parts by mass of water, stir, heat up to 90° C., and perform a gelatinization reaction for 1 hour to obtain a starch paste;
[0036] b, get 1 mass part of chitosan and join in the starch paste, and slowly add 0.2 mass part of crosslinking agent, 0.2 mass part of plasticizer, 0.2 mass part of polyvinyl alcohol, 0.2 mass part of Sodium sulfate, the Tween 60 of 0.1 mass part, obtains mixed material;
[0037] c. React the mixed material at 90° C. for 1 hour, cool to room temperature, let it stand for 2 hours, and defoam to obtain a chitosan-modified starch-type sizing agent.
[0038] The sizing performance test results of Examples 1, 2 and 3 are shown in Table 1 and Table 2 below:
[0039] Table 1: Performance parameters of the wetting agent prepared in Examples 1, 2 and 3
[0040] ...
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