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A synthetic block of colorless diamond for artificial synthetic jewelry and its synthetic method

A technology of artificial synthesis and synthesis method, which is applied in the application of ultra-high pressure process, jewelry, etc., which can solve the problem that the product quality and yield cannot reach industrial production, the structural stability of the synthetic block and the heat preservation effect are poor, and the product purity is poor, etc. problems, to avoid the generation of inclusions or internal impurities, improve the purity and hardness of diamonds, and improve the yield and color level of the effect

Active Publication Date: 2019-01-11
ZHONGNAN DIAMOND CO LTD
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  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although, in recent years, the domestic temperature difference method plus fading synthesis technology has made breakthroughs and can produce a small amount of colorless diamonds, but the structural stability and thermal insulation effect of the synthetic blocks are poor, the nitrogen removal efficiency is low, and the product purity is poor, resulting in product The quality and yield are far from meeting the requirements of industrial production. The color grade is basically G / H grade, and a very small amount of E / F grade. A reliable and stable synthesis method is the basic condition for realizing the industrial production of large-grained colorless diamonds for jewelry.

Method used

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  • A synthetic block of colorless diamond for artificial synthetic jewelry and its synthetic method

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Embodiment Construction

[0019] The present invention will be further described below in combination with specific embodiments.

[0020] see figure 1 , a synthetic block of colorless diamonds for synthetic jewelry of the present invention and a synthetic method thereof, the synthetic block used in the method comprises a pyrophyllite empty block 1, and the inside of the first end and the second end of the pyrophyllite empty block 1 are respectively sleeved with Pyrophyllite ring 2, a conductive plug 8 is set inside the pyrophyllite ring 2, and carbon paper 7 is arranged on the inner wall of the pyrophyllite ring 2 and the conductive plug 8 at the first end and the second end of the pyrophyllite empty block 1, and the pyrophyllite empty block 1 is the first Dolomite outer lining 11, carbon tube 10, magnesium oxide inner lining 9 and a core column with a multi-layer permeable structure are sequentially arranged between the two carbon papers 7 at the end and the second end. The first dolomite sheet 6, th...

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Abstract

The invention discloses a synthesis block and synthesis method of colorless diamonds for artificially synthesized jewelries. The synthesis block of the colorless diamond comprises a pyrophyllite empty block and a core column which is arranged in the center of the synthesis block and is of a multi-layer permeability structure, the core column comprises a dolomite flake, a carbon source, a catalyst flake, a Cu foil-catalyst flake composite layer and a crystal bed which are sequentially stacked from the first end to the second end of the pyrophyllite empty block. The synthesis technology method of the colorless diamonds comprises the steps that by controlling the ingredients of the medium flake, the purity of the carbon source and the thickness of the Cu foil, thermal molecular movement of carbon atoms, melting of the catalyst flake and a reaction generated between the Cu foil and nitrogen atoms mutually achieve synergistic cooperation and achieve combined action appropriately, the carbon atoms make contact with diamond seed crystals to be gaplessly nucleated and grow on the surfaces of the seed crystals, generation of inclusions or internal impurities is avoided, and the purity degree and the hardness level of the diamonds are increased. According to the synthesis block and synthesis method, the product particle size, color and purity degree are guaranteed, the finished product rate and the practicability are high, large-scale production of the pure colorless high-quality diamonds for the jewelries is effectively achieved, and the synthesis block and the synthesis method are worthy of wide application and popularization.

Description

technical field [0001] The invention belongs to the technical field of synthetic production of superhard materials, and relates to a synthetic block of colorless diamonds for artificial synthetic jewelry and a synthetic method thereof, which is suitable for the synthetic production of jewelry-grade colorless diamonds. Background technique [0002] At present, large-grain artificial diamonds have entered the field of jewelry, and large-grain colorless diamonds (Type IIa) for jewelry have great market space and prospects. Although, in recent years, the domestic temperature difference method plus fading synthesis technology has made breakthroughs and can produce a small amount of colorless diamonds, but the structural stability and thermal insulation effect of the synthetic blocks are poor, the nitrogen removal efficiency is low, and the product purity is poor, resulting in product The quality and yield are far from meeting the requirements of industrial production. The color g...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J3/06A44C17/00
CPCA44C17/00B01J3/06
Inventor 刘乾坤易良成赵鹏
Owner ZHONGNAN DIAMOND CO LTD
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