Identification method of Patrinia in traditional Chinese medicine compound
A technology of Patrinia and traditional Chinese medicine, which is applied in the preparation, sampling, and measuring devices of test samples, which can solve the problems of no detection and poor separation effect, and achieve excellent effect, good separation effect, and moderate Rf value Effect
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Embodiment 1
[0049] The identification method of Patrinia in the Chinese medicine compound of the present embodiment is the thin-layer chromatography identification of Patrinia in Longqing Tablets:
[0050] 1. Instruments and reagents
[0051] Patrinia control medicinal materials (National Institute for the Control of Pharmaceutical and Biological Products, batch number: 121271-201201); medicinal materials used in the prescription (purchased from Hebei Anguo Traditional Chinese Medicinal Materials Market); Longqing Tablets (Tianjin Zhongxin Pharmaceutical Group Co., Ltd. Longshunrong Pharmaceutical Factory, specifications: each piece weighs 0.6 g, batch number: 20130226); silica gel G plate (100mm×100mm, Qingdao Ocean Chemical Factory); other reagents are analytically pure.
[0052] 2. Methods and Results
[0053] (1) Preparation of contrast medicinal material solution: get Patrinia reference medicinal material 2g, add water 150ml, decoct for half an hour, filter, filtrate is concentrated...
Embodiment 2
[0061] The identification method of Patrinia in the Chinese medicine compound of the present embodiment is the thin-layer chromatography identification of Patrinia in Qianlieping Capsules:
[0062] 1. Instruments and reagents
[0063] Patrinia control medicinal materials (National Institute for the Control of Pharmaceutical and Biological Products, batch number: 121271-201201); medicinal materials used in prescriptions (purchased in Hebei Anguo Traditional Chinese Medicinal Materials Market); Qianlieping Capsules (Xi’an Qianhe Pharmaceutical Co., Ltd., specification: 0.4g / grain, batch number: 20140702); silica gel G plate (100mm×100mm, Qingdao Ocean Chemical Factory); other reagents were of analytical grade.
[0064] 2. Methods and Results
[0065] (1) Preparation of contrast medicinal material solution: get Patrinia reference medicinal material 2g, add water 150ml, decoct for half an hour, filter, filtrate is concentrated to 30ml, prepare with need testing solution prepara...
Embodiment 3
[0073] The identification method of Patrinia in the Chinese medicine compound of the present embodiment is the thin-layer chromatography identification of Patrinia in Jinmagantai granules:
[0074] 1. Instruments and reagents
[0075] Patrinia reference medicinal material (National Institute for the Control of Pharmaceutical and Biological Products, batch number: 121271-201201); medicinal materials used in the prescription (purchased at Hebei Anguo Traditional Chinese Medicine Market); Jinma Gantai Granules (Guizhou Changshou Changle Pharmaceutical Factory, specifications: 2g per bag (no sucrose), batch number: 20160301); silica gel G plate (100mm×100mm, Qingdao Ocean Chemical Factory); other reagents were of analytical grade.
[0076] 2. Methods and Results
[0077] (1) Preparation of contrast medicinal material solution: get Patrinia reference medicinal material 2g, add water 150ml, decoct for half an hour, filter, filtrate is concentrated to 30ml, prepare with need testing...
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